C₂₁H₁₇FN₄O₂

Base Information

Chemical Name:C₂₁H₁₇FN₄O₂
CAS No.:1194019-95-8
Molecular Formula:C₂₁H₁₇FN₄O₂
Molecular Weight:376.39
Hs Code.:

C<sub>21</sub>H<sub>17</sub>FN<sub>4</sub>O<sub>2</sub>

Synonyms:C₂₁H₁₇FN₄O₂

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Chemical Property of C₂₁H₁₇FN₄O₂

Chemical Property:

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Technology Process of C₂₁H₁₇FN₄O₂

There total 7 articles about C₂₁H₁₇FN₄O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 677306-38-6
1H-indazole-4-carboxylic acid

: 1194019-95-8
C₂₁H₁₇FN₄O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: methanol; toluene / 20 °C

2.1: potassium carbonate / trans-N,N'-dimethyl-1,2-cyclohexyldiamine; copper(l) iodide / 20 - 120 °C / Inert atmosphere; sealed tube

3.1: water; sodium hydroxide / methanol / 1 h / Reflux

3.2: 20 °C / pH 3 - 4

4.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 0.25 h / 20 °C

4.2: 5 h

5.1: triethylamine / bis(benzonitrile)palladium(II) dichloride; 1,1'-bis(diphenylphosphino)ferrocene / 4 h / 140 °C / 11251.1 Torr

6.1: lithium borohydride / tetrahydrofuran / 18 h / Reflux

With lithium borohydride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; potassium carbonate; triethylamine; sodium hydroxide; trans-N,N'-dimethyl-1,2-cyclohexyldiamine; copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; 1,1'-bis(diphenylphosphino)ferrocene; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1194018-56-8
5-({[1-(4-fluoro-phenyl)-1H-indazole-4-carbonyl]-amino}-methyl)-pyridine-2-carboxylic acid ethyl ester

: 1194019-95-8
C₂₁H₁₇FN₄O₂

Guidance literature:: With lithium borohydride; In tetrahydrofuran; for 18h; Reflux;

Reference yield:

: 352-34-1
4-fluoro-1-iodobenzene

: 1194019-95-8
C₂₁H₁₇FN₄O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / trans-N,N'-dimethyl-1,2-cyclohexyldiamine; copper(l) iodide / 20 - 120 °C / Inert atmosphere; sealed tube

2.1: water; sodium hydroxide / methanol / 1 h / Reflux

2.2: 20 °C / pH 3 - 4

3.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 0.25 h / 20 °C

3.2: 5 h

4.1: triethylamine / bis(benzonitrile)palladium(II) dichloride; 1,1'-bis(diphenylphosphino)ferrocene / 4 h / 140 °C / 11251.1 Torr

5.1: lithium borohydride / tetrahydrofuran / 18 h / Reflux

With lithium borohydride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; potassium carbonate; triethylamine; sodium hydroxide; trans-N,N'-dimethyl-1,2-cyclohexyldiamine; copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; 1,1'-bis(diphenylphosphino)ferrocene; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;