C₂₉H₃₅NO₂Si

Base Information

• Chemical Name: C₂₉H₃₅NO₂Si
• CAS No.: 1003047-69-5
• Molecular Formula: C₂₉H₃₅NO₂Si
• Molecular Weight: 457.688
• Mol file: 1003047-69-5.mol

Synonyms:C₂₉H₃₅NO₂Si

Chemical Property of C₂₉H₃₅NO₂Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₂₉H₃₅NO₂Si

There total 4 articles about C₂₉H₃₅NO₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

C31H37NO3Si (1021183-57-2) → C29H35NO2Si (1003047-69-5)

Guidance literature:

With LiAlH; In tetrahydrofuran; at 20 ℃; for 16h;

DOI:10.1055/s-2007-990955

Reference yield:

C26H29NOSi → C29H35NO2Si (1003047-69-5)

Guidance literature:

Multi-step reaction with 4 steps

1: 58 percent / POCl₃ / 1.25 h / 0 - 20 °C

2: 87 percent / ethanol / 48 h / 110 °C

3: 100 percent / H₂ / Pd/C / 8.5 h / 20 °C

4: 88 percent / LiAlH / tetrahydrofuran / 16 h / 20 °C

With hydrogen; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; ethanol; 1: Vilsmeier formilation reaction / 2: Wittig olefination reaction;

DOI:10.1055/s-2007-990955

Reference yield:

C27H29NO2Si (1003047-65-1) → C29H35NO2Si (1003047-69-5)

Guidance literature:

Multi-step reaction with 3 steps

1: 87 percent / ethanol / 48 h / 110 °C

2: 100 percent / H₂ / Pd/C / 8.5 h / 20 °C

3: 88 percent / LiAlH / tetrahydrofuran / 16 h / 20 °C

With hydrogen; palladium on activated charcoal; In tetrahydrofuran; ethanol; 1: Wittig olefination reaction;

DOI:10.1055/s-2007-990955

upstream raw materials:

C₃₁H₃₇NO₃Si

C₂₇H₂₉NO₂Si

C₃₁H₃₅NO₃Si