C₅₄H₆₀N₆O₉

Base Information

Chemical Name:C₅₄H₆₀N₆O₉
CAS No.:1379654-60-0
Molecular Formula:C₅₄H₆₀N₆O₉
Molecular Weight:937.105
Hs Code.:

C<sub>54</sub>H<sub>60</sub>N<sub>6</sub>O<sub>9</sub>

Synonyms:C₅₄H₆₀N₆O₉

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Chemical Property of C₅₄H₆₀N₆O₉

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Technology Process of C₅₄H₆₀N₆O₉

There total 15 articles about C₅₄H₆₀N₆O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₄H₆₂N₆O₁₀

: 1379654-60-0
C₅₄H₆₀N₆O₉

Guidance literature:: C₅₄H₆₂N₆O₁₀; With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-hydroxy-3,4-dihydrobenzotriazine-4-one; In N,N-dimethyl-formamide; at 0 ℃; for 1h;

In N,N-dimethyl-formamide; at 20 ℃; for 96h;
DOI:10.1002/chem.201103185

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 1379654-60-0
C₅₄H₆₀N₆O₉

Guidance literature:: Multi-step reaction with 11 steps

1.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 1 h / 0 °C

1.2: 3 h / 20 °C

2.1: tetrabutylammomium bromide; sodium hydroxide / dichloromethane / 1 h / 20 °C

3.1: trifluoroacetic acid / chloroform / 1 h / 0 °C

4.1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 1 h / 0 °C

4.2: 96 h / 20 °C

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / methanol; water; toluene / 2 h / 90 °C

6.1: tetrabutylammonium hydrogen sulfate / dichloromethane / 2 h / 20 °C

7.1: trifluoroacetic acid / chloroform / 1 h / 0 °C

8.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-hydroxy-3,4-dihydrobenzotriazine-4-one / tetrahydrofuran / 72 h / 0 - 20 °C / Inert atmosphere

9.1: lithium hydroxide monohydrate; dihydrogen peroxide / methanol / 1 h / 0 °C

9.2: 22 h / 20 °C

10.1: trifluoroacetic acid / chloroform / 2 h / 0 °C

11.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-hydroxy-3,4-dihydrobenzotriazine-4-one / N,N-dimethyl-formamide / 1 h / 0 °C

11.2: 96 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1-hydroxy-7-aza-benzotriazole; lithium hydroxide monohydrate; tetrabutylammomium bromide; dihydrogen peroxide; sodium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; 3-hydroxy-3,4-dihydrobenzotriazine-4-one; triphenylphosphine; tetrabutylammonium hydrogen sulfate; trifluoroacetic acid; sodium hydroxide; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; toluene; 5.1: Suzuki coupling;
DOI:10.1002/chem.201103185

Reference yield:

: 691394-91-9
methyl (S)-3-(4-(benzyloxy)-3-iodophenyl)-2-((tert-butoxycarbonyl)amino)propanoate

: 1379654-60-0
C₅₄H₆₀N₆O₉

Guidance literature:: Multi-step reaction with 10 steps

1.1: tetrabutylammomium bromide; sodium hydroxide / dichloromethane / 1 h / 20 °C

2.1: trifluoroacetic acid / chloroform / 1 h / 0 °C

3.1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 1 h / 0 °C

3.2: 96 h / 20 °C

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / methanol; water; toluene / 2 h / 90 °C

5.1: tetrabutylammonium hydrogen sulfate / dichloromethane / 2 h / 20 °C

6.1: trifluoroacetic acid / chloroform / 1 h / 0 °C

7.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-hydroxy-3,4-dihydrobenzotriazine-4-one / tetrahydrofuran / 72 h / 0 - 20 °C / Inert atmosphere

8.1: lithium hydroxide monohydrate; dihydrogen peroxide / methanol / 1 h / 0 °C

8.2: 22 h / 20 °C

9.1: trifluoroacetic acid / chloroform / 2 h / 0 °C

10.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-hydroxy-3,4-dihydrobenzotriazine-4-one / N,N-dimethyl-formamide / 1 h / 0 °C

10.2: 96 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1-hydroxy-7-aza-benzotriazole; lithium hydroxide monohydrate; tetrabutylammomium bromide; dihydrogen peroxide; sodium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; 3-hydroxy-3,4-dihydrobenzotriazine-4-one; tetrabutylammonium hydrogen sulfate; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; toluene; 4.1: Suzuki coupling;
DOI:10.1002/chem.201103185