pentafluorophenyl 2-(pyren-1-yl)acetate

Base Information

Chemical Name:pentafluorophenyl 2-(pyren-1-yl)acetate
CAS No.:197722-93-3
Molecular Formula:C₂₄H₁₁F₅O₂
Molecular Weight:426.342
Hs Code.:

Synonyms:pentafluorophenyl 2-(pyren-1-yl)acetate

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Chemical Property of pentafluorophenyl 2-(pyren-1-yl)acetate

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Technology Process of pentafluorophenyl 2-(pyren-1-yl)acetate

There total 2 articles about pentafluorophenyl 2-(pyren-1-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 64709-55-3
1-pyreneacetic acid

: 197722-93-3
pentafluorophenyl 2-(pyren-1-yl)acetate

Guidance literature:: With dicyclohexyl-carbodiimide; In 1,4-dioxane; ethyl acetate; for 18h;

Reference yield:

: 14533-84-7
pentafluorophenyl trifloroacetate

: 64709-55-3
1-pyreneacetic acid

: 197722-93-3
pentafluorophenyl 2-(pyren-1-yl)acetate

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1039/c4ob00603h

Reference yield:

: 197722-93-3
pentafluorophenyl 2-(pyren-1-yl)acetate

: O¹-(4,4'-dimethoxytrityl)-O³-(N,N-diisopropylamino-2-cyanoethoxyphosphinyl)-4-(1-pyrenyl)-1,3-butanediol

Guidance literature:: Multi-step reaction with 5 steps

1: 94 percent / Et₃N / tetrahydrofuran / 1 h / 20 °C

2: 86 percent / TFA / 0.5 h / Heating

3: 87 percent / NaBH₄ / tetrahydrofuran; methanol / Heating

4: 80 percent / pyridine / 1 h / 20 °C

5: 73 percent / diisopropylaminoum tetrazolide / acetonitrile / 2 h

With pyridine; sodium tetrahydroborate; N,N-diisopropylamine tetrazolide; triethylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; acetonitrile; 1: Condensation / 2: Ring cleavage / 3: Reduction / 4: Substitution / 5: Substitution;
DOI:10.1080/07328319908044632