α,α'-bis(dithiocarboxyoxy)-p-xylene potassium salt

Base Information

Chemical Name:α,α'-bis(dithiocarboxyoxy)-p-xylene potassium salt
CAS No.:73393-33-6
Molecular Formula:C₁₀H₈O₂S₄*2K
Molecular Weight:366.633
Hs Code.:

Synonyms:α,α'-bis(dithiocarboxyoxy)-p-xylene potassium salt

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Chemical Property of α,α'-bis(dithiocarboxyoxy)-p-xylene potassium salt

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Technology Process of α,α'-bis(dithiocarboxyoxy)-p-xylene potassium salt

There total 1 articles about α,α'-bis(dithiocarboxyoxy)-p-xylene potassium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 75-15-0,12122-00-8
carbon disulfide

: 589-29-7
p-xylylene glycol

: 73393-33-6
α,α'-bis(dithiocarboxyoxy)-p-xylene potassium salt

Guidance literature:: With potassium hydroxide; In tetrahydrofuran; at 6 ℃;
DOI:10.1039/c9nj01551e

Reference yield: 86.0%

: 213336-45-9
Ru(CH=CHC₆H₄Me-4)Cl(CO)(2,1,3-benzothiadiazole)(PPh₃)2

: 73393-33-6
α,α'-bis(dithiocarboxyoxy)-p-xylene potassium salt

: [Ru(CH=CHC₆H₄Me-4)(CO)(PPh₃)2]2(S₂COCH₂C₆H₄CH₂COS₂)

Guidance literature:: In methanol; dichloromethane; byproducts: KCl; (under aerobic conditions); Ru-complex in CH2Cl2 stirred with ligand in MeOH at room temp. for 1 h; solvent removed, ppt. dissolved in CH2Cl2, filtered, EtOH added, slowly concd. under reduced pressure, filtered, washed with cold EtOH, hexane, dried under vac.; elem. anal.;
DOI:10.1039/b901822k

Reference yield: 85.0%

: ammonium hexafluorophosphate

: cis-dichlorodi[bis(diphenylphosphino)methane]ruthenium(II)

: 73393-33-6
α,α'-bis(dithiocarboxyoxy)-p-xylene potassium salt

: [Ru(dppm)2]2(S₂COCH₂C₆H₄CH₂COS₂)(PF₆)2

Guidance literature:: In methanol; dichloromethane; byproducts: NH4Cl; (under aerobic conditions); ligand and NH4PF6 in MeOH added to soln. of Ru-complex in CH2Cl2, stirred for 2 h; volatiles removed, ppt. dissolved in CH2Cl2, filtered, EtOH added, slowly concd. under reduced pressure, filtered, washed with cold EtOH, hexane; elem. anal.;
DOI:10.1039/b901822k