4-(hydroxymethyl)phenyl(2E,4E,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,4,6,8-tetraenoate

Base Information

Chemical Name:4-(hydroxymethyl)phenyl(2E,4E,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,4,6,8-tetraenoate
CAS No.:133785-02-1
Molecular Formula:C₂₇H₃₄O₃
Molecular Weight:406.565
Hs Code.:

Synonyms:4-(hydroxymethyl)phenyl(2E,4E,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,4,6,8-tetraenoate

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Chemical Property of 4-(hydroxymethyl)phenyl(2E,4E,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,4,6,8-tetraenoate

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Technology Process of 4-(hydroxymethyl)phenyl(2E,4E,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,4,6,8-tetraenoate

There total 2 articles about 4-(hydroxymethyl)phenyl(2E,4E,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,4,6,8-tetraenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.8%

: 80850-73-3
4-formylphenyl(2E,4E,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,4,6,8-tetraenoate

: 133785-02-1
4-(hydroxymethyl)phenyl(2E,4E,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,4,6,8-tetraenoate

Guidance literature:: With sodium tetrahydroborate; In chloroform; Isopropyl acetate; at 0 ℃; for 1h;
DOI:10.1021/jm8001839

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 133785-02-1
4-(hydroxymethyl)phenyl(2E,4E,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethylcyclohex-1-enyl)nona-2,4,6,8-tetraenoate

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 24 h / 20 °C

2: sodium tetrahydroborate / ipa; chloroform / 1 h / 0 °C

With dmap; sodium tetrahydroborate; dicyclohexyl-carbodiimide; In ipa; chloroform; N,N-dimethyl-formamide;