2-Nitrophenyl2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-a-D-glucopyranoside

Base Information

Chemical Name:2-Nitrophenyl2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-a-D-glucopyranoside
CAS No.:13264-91-0
Molecular Formula:C₂₀H₂₄N₂O₁₁
Molecular Weight:468.417
Hs Code.:
Mol file:13264-91-0.mol

Synonyms:2-Nitrophenyl2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-a-D-glucopyranoside

Suppliers and Price of 2-Nitrophenyl2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-a-D-glucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
o-Nitrophenyl2-Acetamido-2-deoxy-3,4,6-tri-O-acetyl-α-D-glucopyranoside
100mg
$ 285.00

Medical Isotopes, Inc.
2-Nitrophenyl2-acetamido-3-4-6-tri-O-acetyl-2-deoxy-α-D-glucopyranoside
100 mg
$ 663.00

American Custom Chemicals Corporation
2-NITROPHENYL 2-ACETAMIDO-3,4,6-TRI-O-ACETYL-2-DEOXY-ALPHA-D-GLUCOPYRANOSIDE 95.00%
500MG
$ 1871.10

American Custom Chemicals Corporation
2-NITROPHENYL 2-ACETAMIDO-3,4,6-TRI-O-ACETYL-2-DEOXY-ALPHA-D-GLUCOPYRANOSIDE 95.00%
50MG
$ 739.20

Total 10 raw suppliers

Chemical Property of 2-Nitrophenyl2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-a-D-glucopyranoside

Chemical Property:

Melting Point:173-174°C
Boiling Point:649.5±55.0 °C(Predicted)
PKA:13.35±0.70(Predicted)
PSA：172.28000
Density:1.37±0.1 g/cm3(Predicted)
LogP:1.54380

Purity/Quality:

98%,99%, ^*data from raw suppliers

o-Nitrophenyl2-Acetamido-2-deoxy-3,4,6-tri-O-acetyl-α-D-glucopyranoside ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses o-Nitrophenyl 2-Acetamido-2-deoxy-3,4,6-tri-O-acetyl-α-D-glucopyranoside (cas# 13264-91-0) is a compound useful in organic synthesis.

Technology Process of 2-Nitrophenyl2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-a-D-glucopyranoside

There total 8 articles about 2-Nitrophenyl2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-a-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 88-75-5,78813-12-4
2-hydroxynitrobenzene

: 3068-34-6
Acetic acid (2R,3S,4R,5R,6R)-3-acetoxy-2-acetoxymethyl-5-acetylamino-6-chloro-tetrahydro-pyran-4-yl ester

: 13089-26-4,13264-91-0
o-nitrophenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With 15-crown-5; sodium hydrogencarbonate; In acetonitrile; at 20 ℃;
DOI:10.1023/A:1012988719296

Reference yield: 22.0%

: 4148-73-6,13089-19-5,13089-21-9,13089-43-5,13089-70-8,23646-65-3,30657-66-0
phenyl 2-acetamido-2-deoxy-3,4,6-tri-O-acetyl-α-D-mannopyranoside

: 1379001-47-4,13264-91-0
C₂₀H₂₄N₂O₁₁

: 570412-09-8,13089-23-1
4-nitrophenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-mannopyranoside

Guidance literature:: With nitric acid; In acetic anhydride; acetic acid; at 0 - 20 ℃; Cooling with ice;
DOI:10.3762/bjoc.8.48

Reference yield:

: 10378-06-0,20757-53-3,35954-65-5,123483-77-2,134308-33-1
2-methyl-(3,4,6-tri-O-acetyl-1,2-dideoxy-β-D-mannopyrano)-[2,1:4',5']-2-oxazoline

: 1379001-47-4,13264-91-0
C₂₀H₂₄N₂O₁₁

Guidance literature:: Multi-step reaction with 2 steps

1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 72 h / 20 °C

2: nitric acid / acetic anhydride; acetic acid / 0 - 20 °C / Cooling with ice

With trimethylsilyl trifluoromethanesulfonate; nitric acid; In dichloromethane; acetic anhydride; acetic acid;
DOI:10.3762/bjoc.8.48