<2S-(2α(R^*,R^*),3aα,4β,7β,7aα)>-β-(Octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yloxy)-α-phenylbenzolethanol

Base Information

• Chemical Name: <2S-(2α(R^*,R^*),3aα,4β,7β,7aα)>-β-(Octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yloxy)-α-phenylbenzolethanol
• CAS No.: 113775-65-8
• Molecular Formula: C₂₆H₃₂O₃
• Molecular Weight: 392.538

Synonyms:<2S-(2α(R^*,R^*),3aα,4β,7β,7aα)>-β-(Octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yloxy)-α-phenylbenzolethanol

Chemical Property of <2S-(2α(R^*,R^*),3aα,4β,7β,7aα)>-β-(Octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yloxy)-α-phenylbenzolethanol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of <2S-(2α(R^*,R^*),3aα,4β,7β,7aα)>-β-(Octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yloxy)-α-phenylbenzolethanol

There total 4 articles about <2S-(2α(R^*,R^*),3aα,4β,7β,7aα)>-β-(Octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yloxy)-α-phenylbenzolethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

DL-1,2-diphenylethane-1,2-diol (655-48-1) + <2R-(2α,3aα,4β,7β,7aα)>-Octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-ol (108031-76-1) → <2S-(2α(S*,S*),3aα,4β,7β,7aα)>-β-(Octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yloxy)-α-phenylbenzoethanol (113775-64-7) + <2S-(2α(R*,R*),3aα,4β,7β,7aα)>-β-(Octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yloxy)-α-phenylbenzolethanol (113775-65-8)

Guidance literature:

With toluene-4-sulfonic acid; In dichloromethane; for 2h; Ambient temperature;

Reference yield:

1,2-diphenyl-1,2-ethanediol (492-70-6,655-48-1,2325-10-2,38270-73-4,52340-78-0,579-43-1) + <2S-(2α,3aα,4α,7α,7aα)>-2,3,3a,4,5,6,7,7a-Octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-ol (81925-09-9) → <2R-(2α(S*,S*),3aα,4α,7α,7aα)>-2-(7,8,8-Trimethyl-octahydro-4,7-methano-1-benzofuran-2-yloxy)-1,2-diphenylethanol (87218-36-8,87248-57-5,100680-93-1,100680-94-2,113775-64-7,113775-65-8) + (R)-1,2-Diphenyl-2-((1R,2S,4R,6S,7R)-1,10,10-trimethyl-3-oxa-tricyclo[5.2.1.02,6]dec-4-yloxy)-ethanol (87218-36-8,87248-57-5,100680-93-1,100680-94-2,113775-64-7,113775-65-8)

Guidance literature:

With toluene-4-sulfonic acid; triethylamine; Yield given. Multistep reaction. Yields of byproduct given; 1.) CH₂Cl₂, room temp., 1 h;

Reference yield:

1,2-diphenyl-1,2-ethanediol (492-70-6,655-48-1,2325-10-2,38270-73-4,52340-78-0,579-43-1) + <2S-(2α,3aα,4α,7α,7aα)>-2,3,3a,4,5,6,7,7a-Octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-ol (81925-09-9) → <2R-(2α(S*,S*),3aα,4α,7α,7aα)>-2-(7,8,8-Trimethyl-octahydro-4,7-methano-1-benzofuran-2-yloxy)-1,2-diphenylethanol (87218-36-8,87248-57-5,100680-93-1,100680-94-2,113775-64-7,113775-65-8) + (R)-1,2-Diphenyl-2-((1R,2S,4R,6S,7R)-1,10,10-trimethyl-3-oxa-tricyclo[5.2.1.02,6]dec-4-yloxy)-ethanol (87218-36-8,87248-57-5,100680-93-1,100680-94-2,113775-64-7,113775-65-8)

Guidance literature:

With toluene-4-sulfonic acid; triethylamine; Yield given. Multistep reaction. Yields of byproduct given; 1.) CH₂Cl₂, room temp., 1 h;

upstream raw materials:

1,2-diphenyl-1,2-ethanediol

<2S-(2α,3aα,4α,7α,7aα)>-2,3,3a,4,5,6,7,7a-Octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-ol

DL-1,2-diphenylethane-1,2-diol

<2R-(2α,3aα,4β,7β,7aα)>-Octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-ol

Downstream raw materials:

*,R^*)>-1,2-Diphenyl-1,2-ethandiol

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