1,3-DI-MORPHOLIN-4-YL-PROPANE-1,3-DIONE

Base Information

• Chemical Name: 1,3-DI-MORPHOLIN-4-YL-PROPANE-1,3-DIONE
• CAS No.: 10256-01-6
• Molecular Formula: C11H18 N2 O4
• Molecular Weight: 242.27
• Hs Code.: 2934999090
• Mol file: 10256-01-6.mol

Synonyms:Morpholine,4,4'-malonyldi- (7CI); Malonic acid dimorpholide; NSC 93941

Chemical Property of 1,3-DI-MORPHOLIN-4-YL-PROPANE-1,3-DIONE

Chemical Property:

• Vapor Pressure: 1.64E-09mmHg at 25°C
• Boiling Point: 483.7°Cat760mmHg
• Flash Point: 246.3°C
• PSA: 59.08000
• Density: 1.245g/cm³
• LogP: -1.03010

Purity/Quality:

97% ^*data from raw suppliers

1,3-Dimorpholino-1,3-propanedione ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of 1,3-DI-MORPHOLIN-4-YL-PROPANE-1,3-DIONE

There total 6 articles about 1,3-DI-MORPHOLIN-4-YL-PROPANE-1,3-DIONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,4'-<2-<(2-nitrofenil)tio>malonil>dimorfolina (117410-74-9) → 4,4 '-(1,3-dioxo-1,3-propanediyl)dimorpholine (10256-01-6) + 4,4'-<2-<(2-amminofenil)tio>malonil>dimorfolina (117378-57-1)

Guidance literature:

With hydrogen; palladium on activated charcoal; In tetrahydrofuran; under 2280 Torr; Ambient temperature;

Reference yield:

morpholine (110-91-8,99108-56-2) + malonoyl dichloride (1663-67-8) → 4,4 '-(1,3-dioxo-1,3-propanediyl)dimorpholine (10256-01-6)

Guidance literature:

In chloroform;

Reference yield:

morpholine (110-91-8,99108-56-2) + 4,4',4''-(2-oxo-propane-1,1,3-tricarbonyl)-tris-morpholine (100626-07-1) → 4,4 '-(1,3-dioxo-1,3-propanediyl)dimorpholine (10256-01-6)

Guidance literature:

DOI:10.1039/jr9530002251

upstream raw materials:

morpholine

4,4',4''-(2-oxo-propane-1,1,3-tricarbonyl)-tris-morpholine

diethyl malonate

malonoyl dichloride

Downstream raw materials:

4,4'-<2-(2-nitrofenossi)malonil>dimorfolina

4,4'-<2-(2-amminofenossi)malonil>dimorfolina

4,4'-<2-<(2-amminofenil)tio>malonil>dimorfolina

Dithiomalonsaeuredimorpholid