1-benzyloxycarbonylamino-2,3-dimethoxy-5-(2-trimethylsilylethoxy)carbonylaminobenzene

Base Information

Chemical Name:1-benzyloxycarbonylamino-2,3-dimethoxy-5-(2-trimethylsilylethoxy)carbonylaminobenzene
CAS No.:137022-84-5
Molecular Formula:C₂₂H₃₀N₂O₆Si
Molecular Weight:446.575
Hs Code.:

Synonyms:1-benzyloxycarbonylamino-2,3-dimethoxy-5-(2-trimethylsilylethoxy)carbonylaminobenzene

Suppliers and Price of 1-benzyloxycarbonylamino-2,3-dimethoxy-5-(2-trimethylsilylethoxy)carbonylaminobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-benzyloxycarbonylamino-2,3-dimethoxy-5-(2-trimethylsilylethoxy)carbonylaminobenzene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-benzyloxycarbonylamino-2,3-dimethoxy-5-(2-trimethylsilylethoxy)carbonylaminobenzene

There total 7 articles about 1-benzyloxycarbonylamino-2,3-dimethoxy-5-(2-trimethylsilylethoxy)carbonylaminobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22027-96-9
5-nitroveratral

: 137022-84-5
1-benzyloxycarbonylamino-2,3-dimethoxy-5-(2-trimethylsilylethoxy)carbonylaminobenzene

Guidance literature:: Multi-step reaction with 7 steps

1: iron dust, 12 M HCl / methanol / 10 h / Heating

2: Na₂CO₃ / diethyl ether; H₂O / 1.) 0 deg C, 30 min; 2.) room temp., 2 h

3: 93 percent / Jones reagent / acetone / 1.) 0 deg C, 30 min; 2.) room temp., 1 h

4: tetrahydrofuran / 2 h / Ambient temperature

5: 2 M aq. NaN₃ / tetrahydrofuran; H₂O / 2 h / Ambient temperature

6: toluene / 0.5 h / Heating

7: toluene / 2 h / 60 °C

With hydrogenchloride; sodium azide; jones reagent; iron; sodium carbonate; In tetrahydrofuran; methanol; diethyl ether; water; acetone; toluene;
DOI:10.1016/S0040-4020(01)85065-1

Reference yield:

: 3-amino-4,5-dimethoxy-benzaldehyde

: 137022-84-5
1-benzyloxycarbonylamino-2,3-dimethoxy-5-(2-trimethylsilylethoxy)carbonylaminobenzene

Guidance literature:: Multi-step reaction with 6 steps

1: Na₂CO₃ / diethyl ether; H₂O / 1.) 0 deg C, 30 min; 2.) room temp., 2 h

2: 93 percent / Jones reagent / acetone / 1.) 0 deg C, 30 min; 2.) room temp., 1 h

3: tetrahydrofuran / 2 h / Ambient temperature

4: 2 M aq. NaN₃ / tetrahydrofuran; H₂O / 2 h / Ambient temperature

5: toluene / 0.5 h / Heating

6: toluene / 2 h / 60 °C

With sodium azide; jones reagent; sodium carbonate; In tetrahydrofuran; diethyl ether; water; acetone; toluene;
DOI:10.1016/S0040-4020(01)85065-1

Reference yield:

: 155989-60-9
3-Benzyloxycarbonylamino-4,5-dimethoxy-benzoic acid

: 137022-84-5
1-benzyloxycarbonylamino-2,3-dimethoxy-5-(2-trimethylsilylethoxy)carbonylaminobenzene

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / 2 h / Ambient temperature

2: 2 M aq. NaN₃ / tetrahydrofuran; H₂O / 2 h / Ambient temperature

3: toluene / 0.5 h / Heating

4: toluene / 2 h / 60 °C

With sodium azide; In tetrahydrofuran; water; toluene;
DOI:10.1016/S0040-4020(01)85065-1