(S)-tert-butyl (3-3-(((2E)-3-methoxy-2-methylprop-2-enoyl)carbamoyl)amino)piperidine-1-carboxylate

Base Information

Chemical Name:(S)-tert-butyl (3-3-(((2E)-3-methoxy-2-methylprop-2-enoyl)carbamoyl)amino)piperidine-1-carboxylate
CAS No.:1395795-28-4
Molecular Formula:C₁₆H₂₇N₃O₅
Molecular Weight:341.407
Hs Code.:

Synonyms:(S)-tert-butyl (3-3-(((2E)-3-methoxy-2-methylprop-2-enoyl)carbamoyl)amino)piperidine-1-carboxylate

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Chemical Property of (S)-tert-butyl (3-3-(((2E)-3-methoxy-2-methylprop-2-enoyl)carbamoyl)amino)piperidine-1-carboxylate

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Technology Process of (S)-tert-butyl (3-3-(((2E)-3-methoxy-2-methylprop-2-enoyl)carbamoyl)amino)piperidine-1-carboxylate

There total 1 articles about (S)-tert-butyl (3-3-(((2E)-3-methoxy-2-methylprop-2-enoyl)carbamoyl)amino)piperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52410-41-0,114274-71-4
3-methoxy-2-methylacryloyl chloride

: 3315-16-0
silver cyanate

: 625471-18-3
tert-butyl (3S)-3-aminopiperidine-1-carboxylate

: 1395795-28-4
(S)-tert-butyl (3-3-(((2E)-3-methoxy-2-methylprop-2-enoyl)carbamoyl)amino)piperidine-1-carboxylate

Guidance literature:: 3-methoxy-2-methylacryloyl chloride; silver cyanate; In toluene; at 95 ℃; for 3h;

tert-butyl (3S)-3-aminopiperidine-1-carboxylate; In N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1021/jm3011806

Reference yield:

: 1395795-28-4
(S)-tert-butyl (3-3-(((2E)-3-methoxy-2-methylprop-2-enoyl)carbamoyl)amino)piperidine-1-carboxylate

: C₃₁H₃₇ClN₄O₃

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid / water; 1,4-dioxane / 16 h / 95 °C

2: N-ethyl-N,N-diisopropylamine / acetonitrile / 20 h / 70 °C

3: potassium carbonate / 1-methyl-pyrrolidin-2-one / 0.5 h / 150 °C / Microwave irradiation

With sulfuric acid; potassium carbonate; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; 1-methyl-pyrrolidin-2-one; water; acetonitrile;
DOI:10.1021/jm3011806

Reference yield:

: 1395795-28-4
(S)-tert-butyl (3-3-(((2E)-3-methoxy-2-methylprop-2-enoyl)carbamoyl)amino)piperidine-1-carboxylate

: C₃₁H₃₅ClN₄O₃

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid / water; 1,4-dioxane / 16 h / 95 °C

2: N-ethyl-N,N-diisopropylamine / acetonitrile / 20 h / 70 °C

3: potassium carbonate / 1-methyl-pyrrolidin-2-one / 0.5 h / 150 °C / Microwave irradiation

With sulfuric acid; potassium carbonate; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; 1-methyl-pyrrolidin-2-one; water; acetonitrile;
DOI:10.1021/jm3011806