C₂₇H₂₁NO₆

Base Information

Chemical Name:C₂₇H₂₁NO₆
CAS No.:1375467-90-5
Molecular Formula:C₂₇H₂₁NO₆
Molecular Weight:455.467
Hs Code.:

C<sub>27</sub>H<sub>21</sub>NO<sub>6</sub>

Synonyms:C₂₇H₂₁NO₆

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Chemical Property of C₂₇H₂₁NO₆

Chemical Property:

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Technology Process of C₂₇H₂₁NO₆

There total 5 articles about C₂₇H₂₁NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1375467-87-0
C₃₆H₄₁NO₆Si

: 33458-77-4
7,14-dihydro-12bH-[1,3]dioxolo[4,5-i][1,3]dioxolo[4',5':4,5]benzo[1,2-c]phenanthridine-13-carboxylic acid benzyl ester

: 1375467-90-5
C₂₇H₂₁NO₆

Guidance literature:: C₃₆H₄₁NO₆Si; In acetonitrile; at 80 ℃; for 1h; Inert atmosphere;

In 5,5-dimethyl-1,3-cyclohexadiene; acetonitrile; at 120 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol300967a

Reference yield:

: 1375467-83-6
C₁₉H₂₆O₃Si

: 33458-77-4
7,14-dihydro-12bH-[1,3]dioxolo[4,5-i][1,3]dioxolo[4',5':4,5]benzo[1,2-c]phenanthridine-13-carboxylic acid benzyl ester

: 1375467-90-5
C₂₇H₂₁NO₆

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylsilane; trifluoroacetic acid / acetonitrile / 18 h / 0 - 20 °C / Inert atmosphere

2.1: copper(l) iodide; caesium carbonate; N,N`-dimethylethylenediamine / tetrahydrofuran / 87 h / 80 °C / Inert atmosphere

3.1: tetrabutylammonium triphenyldifluorosilicate / 1,4-dioxane / 96 h / 20 °C / Inert atmosphere

4.1: acetonitrile / 1 h / 80 °C / Inert atmosphere

4.2: 1 h / 120 °C / Inert atmosphere

With triethylsilane; copper(l) iodide; caesium carbonate; tetrabutylammonium triphenyldifluorosilicate; trifluoroacetic acid; N,N`-dimethylethylenediamine; In tetrahydrofuran; 1,4-dioxane; acetonitrile; 4.2: Diels-Alder reaction;
DOI:10.1021/ol300967a

Reference yield:

: 1375467-84-7
C₂₇H₃₅NO₄Si

: 33458-77-4
7,14-dihydro-12bH-[1,3]dioxolo[4,5-i][1,3]dioxolo[4',5':4,5]benzo[1,2-c]phenanthridine-13-carboxylic acid benzyl ester

: 1375467-90-5
C₂₇H₂₁NO₆

Guidance literature:: Multi-step reaction with 3 steps

1.1: copper(l) iodide; caesium carbonate; N,N`-dimethylethylenediamine / tetrahydrofuran / 87 h / 80 °C / Inert atmosphere

2.1: tetrabutylammonium triphenyldifluorosilicate / 1,4-dioxane / 96 h / 20 °C / Inert atmosphere

3.1: acetonitrile / 1 h / 80 °C / Inert atmosphere

3.2: 1 h / 120 °C / Inert atmosphere

With copper(l) iodide; caesium carbonate; tetrabutylammonium triphenyldifluorosilicate; N,N`-dimethylethylenediamine; In tetrahydrofuran; 1,4-dioxane; acetonitrile; 3.2: Diels-Alder reaction;
DOI:10.1021/ol300967a