5'-O--5-<<2-<<2-<<(2,2-dimethylethoxy)carbonyl>amino>-3-<1-<(2,2-dimethylethoxy)carbonyl>-1H-imidazol-4-yl>-1-oxopropyl>amino>ethyl>thio>-2'-deoxyuridine

Base Information

Chemical Name:5'-O--5-<<2-<<2-<<(2,2-dimethylethoxy)carbonyl>amino>-3-<1-<(2,2-dimethylethoxy)carbonyl>-1H-imidazol-4-yl>-1-oxopropyl>amino>ethyl>thio>-2'-deoxyuridine
CAS No.:128870-26-8
Molecular Formula:C₄₈H₅₈N₆O₁₂S
Molecular Weight:943.088
Hs Code.:

5'-O-<Bis(4-methoxyphenyl)phenylmethyl>-5-<<2-<<2-<<(2,2-dimethylethoxy)carbonyl>amino>-3-<1-<(2,2-dimethylethoxy)carbonyl>-1H-imidazol-4-yl>-1-oxopropyl>amino>ethyl>thio>-2'-deoxyuridine

Synonyms:5'-O--5-<<2-<<2-<<(2,2-dimethylethoxy)carbonyl>amino>-3-<1-<(2,2-dimethylethoxy)carbonyl>-1H-imidazol-4-yl>-1-oxopropyl>amino>ethyl>thio>-2'-deoxyuridine

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Chemical Property of 5'-O--5-<<2-<<2-<<(2,2-dimethylethoxy)carbonyl>amino>-3-<1-<(2,2-dimethylethoxy)carbonyl>-1H-imidazol-4-yl>-1-oxopropyl>amino>ethyl>thio>-2'-deoxyuridine

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Technology Process of 5'-O--5-<<2-<<2-<<(2,2-dimethylethoxy)carbonyl>amino>-3-<1-<(2,2-dimethylethoxy)carbonyl>-1H-imidazol-4-yl>-1-oxopropyl>amino>ethyl>thio>-2'-deoxyuridine

There total 4 articles about 5'-O--5-<<2-<<2-<<(2,2-dimethylethoxy)carbonyl>amino>-3-<1-<(2,2-dimethylethoxy)carbonyl>-1H-imidazol-4-yl>-1-oxopropyl>amino>ethyl>thio>-2'-deoxyuridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: pentafluorophenyl ester of di-tert-butoxycarbonylhistidine

: 128870-25-7
5'-O-DMT-5-<(2-aminoethyl)thio>-2'-deoxyuridine

: 128870-26-8
5'-O--5-<<2-<<2-<<(2,2-dimethylethoxy)carbonyl>amino>-3-<1-<(2,2-dimethylethoxy)carbonyl>-1H-imidazol-4-yl>-1-oxopropyl>amino>ethyl>thio>-2'-deoxyuridine

Guidance literature:: With triethylamine; In dichloromethane; for 3h; Ambient temperature;
DOI:10.1021/jo00304a026

Reference yield:

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 128870-26-8
5'-O--5-<<2-<<2-<<(2,2-dimethylethoxy)carbonyl>amino>-3-<1-<(2,2-dimethylethoxy)carbonyl>-1H-imidazol-4-yl>-1-oxopropyl>amino>ethyl>thio>-2'-deoxyuridine

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 3.5 h / Ambient temperature

2: NH₃ / 24 h

3: 77 percent / Et₃N / CH₂Cl₂ / 3 h / Ambient temperature

With pyridine; ammonia; triethylamine; In dichloromethane;
DOI:10.1021/jo00304a026

Reference yield:

: 118042-45-8
5-<3-(Trifluoroacetamido)-1-thiapropyl>-2'-deoxyuridine

: 128870-26-8
5'-O--5-<<2-<<2-<<(2,2-dimethylethoxy)carbonyl>amino>-3-<1-<(2,2-dimethylethoxy)carbonyl>-1H-imidazol-4-yl>-1-oxopropyl>amino>ethyl>thio>-2'-deoxyuridine

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 3.5 h / Ambient temperature

2: NH₃ / 24 h

3: 77 percent / Et₃N / CH₂Cl₂ / 3 h / Ambient temperature

With pyridine; ammonia; triethylamine; In dichloromethane;
DOI:10.1021/jo00304a026