phenylglyoxylic acid 1-adamantyl ester

Base Information

Chemical Name:phenylglyoxylic acid 1-adamantyl ester
CAS No.:899452-03-0
Molecular Formula:C₁₈H₂₀O₃
Molecular Weight:284.355
Hs Code.:

Synonyms:phenylglyoxylic acid 1-adamantyl ester

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Chemical Property of phenylglyoxylic acid 1-adamantyl ester

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Technology Process of phenylglyoxylic acid 1-adamantyl ester

There total 2 articles about phenylglyoxylic acid 1-adamantyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 25726-04-9
phenylglyoxylyl chloride

: 768-95-6
1-adamanthanol

: 899452-03-0
phenylglyoxylic acid 1-adamantyl ester

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1016/j.jcat.2006.04.027

Reference yield:

: 611-73-4
Benzoylformic acid

: 899452-03-0
phenylglyoxylic acid 1-adamantyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride; DMF / CH₂Cl₂ / 4 h / 20 °C

2: 4-dimethylaminopyridine; triethylamine / CH₂Cl₂ / 24 h / 20 °C

With dmap; oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1016/j.jcat.2006.04.027