N-((1H-benzo[d]imidazol-2-yl)methyl)-N-benzyl-4-((benzylamino)-methyl)benzenesulfonamide trifluoroacetate

Base Information

Chemical Name:N-((1H-benzo[d]imidazol-2-yl)methyl)-N-benzyl-4-((benzylamino)-methyl)benzenesulfonamide trifluoroacetate
CAS No.:1057447-16-1
Molecular Formula:C₂HF₃O₂*C₂₉H₂₈N₄O₂S
Molecular Weight:610.657
Hs Code.:

Synonyms:N-((1H-benzo[d]imidazol-2-yl)methyl)-N-benzyl-4-((benzylamino)-methyl)benzenesulfonamide trifluoroacetate

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Chemical Property of N-((1H-benzo[d]imidazol-2-yl)methyl)-N-benzyl-4-((benzylamino)-methyl)benzenesulfonamide trifluoroacetate

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Technology Process of N-((1H-benzo[d]imidazol-2-yl)methyl)-N-benzyl-4-((benzylamino)-methyl)benzenesulfonamide trifluoroacetate

There total 6 articles about N-((1H-benzo[d]imidazol-2-yl)methyl)-N-benzyl-4-((benzylamino)-methyl)benzenesulfonamide trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1057490-22-8
N-((1H-benzo[d]imidazol-2-yl)methyl)-N-benzyl-4-formylbenzenesulfonamide

: 100-46-9
benzylamine

: 1057447-16-1
N-((1H-benzo[d]imidazol-2-yl)methyl)-N-benzyl-4-((benzylamino)-methyl)benzenesulfonamide trifluoroacetate

Guidance literature:: N-((1H-benzo[d]imidazol-2-yl)methyl)-N-benzyl-4-formylbenzenesulfonamide; benzylamine; acetic acid; In 1,2-dichloro-ethane; at 20 ℃; for 0.25h;

With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 60 ℃; for 1.5h;

With trifluoroacetic acid; In 1,2-dichloro-ethane;

Reference yield:

: 4857-04-9
2-chloromethyl-1H-benzimidazole

: 1057447-16-1
N-((1H-benzo[d]imidazol-2-yl)methyl)-N-benzyl-4-((benzylamino)-methyl)benzenesulfonamide trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: dmap / tetrahydrofuran / 2 h / 60 °C

2.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 18 h / 60 °C

3.1: acetic acid / 1,2-dichloro-ethane / 0.25 h / 20 °C

3.2: 1.5 h / 60 °C

With dmap; potassium carbonate; potassium iodide; acetic acid; In tetrahydrofuran; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

: N-benzyl-4-formylbenzenesulfonamide

: 1057447-16-1
N-((1H-benzo[d]imidazol-2-yl)methyl)-N-benzyl-4-((benzylamino)-methyl)benzenesulfonamide trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 18 h / 60 °C

2.1: acetic acid / 1,2-dichloro-ethane / 0.25 h / 20 °C

2.2: 1.5 h / 60 °C

With potassium carbonate; potassium iodide; acetic acid; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;