-1-(4,8-dithiaspiro<2.5>oct-1-yl)-2-(triphenylmethoxy)ethanol

Base Information

Chemical Name:-1-(4,8-dithiaspiro<2.5>oct-1-yl)-2-(triphenylmethoxy)ethanol
CAS No.:135619-08-8
Molecular Formula:C₂₇H₂₈O₂S₂
Molecular Weight:448.65
Hs Code.:

<S-(R*,R*)>-1-(4,8-dithiaspiro<2.5>oct-1-yl)-2-(triphenylmethoxy)ethanol

Synonyms:-1-(4,8-dithiaspiro<2.5>oct-1-yl)-2-(triphenylmethoxy)ethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of -1-(4,8-dithiaspiro<2.5>oct-1-yl)-2-(triphenylmethoxy)ethanol

Chemical Property:

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Technology Process of -1-(4,8-dithiaspiro<2.5>oct-1-yl)-2-(triphenylmethoxy)ethanol

There total 5 articles about -1-(4,8-dithiaspiro<2.5>oct-1-yl)-2-(triphenylmethoxy)ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 135598-40-2
3,4-anhydro-2-deoxy-5-O-(triphenylmethyl)-D-threo-pentose cyclic 1,3-propanediyl mercaptal

: 135619-08-8
-1-(4,8-dithiaspiro<2.5>oct-1-yl)-2-(triphenylmethoxy)ethanol

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at 20 ℃; for 3h;
DOI:10.1021/jo00021a015

Reference yield:

: 452-51-7,13046-70-3,29780-54-9,36792-87-7,36792-88-8,113890-35-0,113890-38-3
D-2-deoxyribose

: 135619-08-8
-1-(4,8-dithiaspiro<2.5>oct-1-yl)-2-(triphenylmethoxy)ethanol

Guidance literature:: Multi-step reaction with 5 steps

1: 89.5 percent / 6 N HCl / CHCl₃ / 4 h / 20 °C

2: 81 percent / pyridine / 24 h / 20 °C

3: 1.35 g / pyridine / 48 h / 20 °C

4: 98 percent / 1 N MeONa / methanol / 3 h

5: 74 percent / n-BuLi / tetrahydrofuran; hexane / 3 h / 20 °C

With pyridine; hydrogenchloride; n-butyllithium; sodium methylate; In tetrahydrofuran; methanol; hexane; chloroform;
DOI:10.1021/jo00021a015

Reference yield:

: 50907-65-8
2-deoxy-D-erythro-pentose cyclic 1,3-propanediyl mercaptal

: 135619-08-8
-1-(4,8-dithiaspiro<2.5>oct-1-yl)-2-(triphenylmethoxy)ethanol

Guidance literature:: Multi-step reaction with 4 steps

1: 81 percent / pyridine / 24 h / 20 °C

2: 1.35 g / pyridine / 48 h / 20 °C

3: 98 percent / 1 N MeONa / methanol / 3 h

4: 74 percent / n-BuLi / tetrahydrofuran; hexane / 3 h / 20 °C

With pyridine; n-butyllithium; sodium methylate; In tetrahydrofuran; methanol; hexane;
DOI:10.1021/jo00021a015