(4S,14S)-(+)-3,15-dimethyl-4,14-diphenyl-6,9,12-trioxa-3,15,21-triazabicyclo<15.3.1>heneicosa-1(21),17,19-triene-2,16-dione

Base Information

Chemical Name:(4S,14S)-(+)-3,15-dimethyl-4,14-diphenyl-6,9,12-trioxa-3,15,21-triazabicyclo<15.3.1>heneicosa-1(21),17,19-triene-2,16-dione
CAS No.:143331-32-2
Molecular Formula:C₂₉H₃₃N₃O₅
Molecular Weight:503.598
Hs Code.:

Synonyms:(4S,14S)-(+)-3,15-dimethyl-4,14-diphenyl-6,9,12-trioxa-3,15,21-triazabicyclo<15.3.1>heneicosa-1(21),17,19-triene-2,16-dione

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Chemical Property of (4S,14S)-(+)-3,15-dimethyl-4,14-diphenyl-6,9,12-trioxa-3,15,21-triazabicyclo<15.3.1>heneicosa-1(21),17,19-triene-2,16-dione

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Technology Process of (4S,14S)-(+)-3,15-dimethyl-4,14-diphenyl-6,9,12-trioxa-3,15,21-triazabicyclo<15.3.1>heneicosa-1(21),17,19-triene-2,16-dione

There total 3 articles about (4S,14S)-(+)-3,15-dimethyl-4,14-diphenyl-6,9,12-trioxa-3,15,21-triazabicyclo<15.3.1>heneicosa-1(21),17,19-triene-2,16-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 3739-94-4
2,6-Pyridinedicarbonyl dichloride

: 143331-37-7
(3S,13S)-(+)-3,13-diphenyl-2,14-diaza-5,8,11-trioxapentadecane

: 143331-32-2
(4S,14S)-(+)-3,15-dimethyl-4,14-diphenyl-6,9,12-trioxa-3,15,21-triazabicyclo<15.3.1>heneicosa-1(21),17,19-triene-2,16-dione

Guidance literature:: With triethylamine; In toluene; for 24h; Ambient temperature;
DOI:10.1021/jo00046a020

Reference yield:

: 143394-36-9
C₂₉H₃₃N₃O₅*C₁₂H₁₃N*ClHO₄

: 82431-48-9
(S)-α-(1-naphthyl)ethylammonium perchlorate

: 143331-32-2
(4S,14S)-(+)-3,15-dimethyl-4,14-diphenyl-6,9,12-trioxa-3,15,21-triazabicyclo<15.3.1>heneicosa-1(21),17,19-triene-2,16-dione

Guidance literature:: In nitromethane-d3; at 20 ℃; Equilibrium constant; Thermodynamic data; free energy of activation in CD₂Cl₂;
DOI:10.1021/jo00046a020

Reference yield:

: 143394-35-8
C₂₉H₃₃N₃O₅*C₁₂H₁₃N*ClHO₄

: 82456-17-5
(R)-α-(1-naphthyl)ethylamine perchlorate salt

: 143331-32-2
(4S,14S)-(+)-3,15-dimethyl-4,14-diphenyl-6,9,12-trioxa-3,15,21-triazabicyclo<15.3.1>heneicosa-1(21),17,19-triene-2,16-dione

Guidance literature:: In nitromethane-d3; at 20 ℃; Equilibrium constant; Thermodynamic data; free energy of activation in CD₂Cl₂;
DOI:10.1021/jo00046a020