(S)-2-[4-(2-Benzyloxycarbonylamino-acetylamino)-benzoylamino]-pentanedioic acid di-tert-butyl ester

Base Information

Chemical Name:(S)-2-[4-(2-Benzyloxycarbonylamino-acetylamino)-benzoylamino]-pentanedioic acid di-tert-butyl ester
CAS No.:162877-46-5
Molecular Formula:C₃₀H₃₉N₃O₈
Molecular Weight:569.655
Hs Code.:

Synonyms:(S)-2-[4-(2-Benzyloxycarbonylamino-acetylamino)-benzoylamino]-pentanedioic acid di-tert-butyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-[4-(2-Benzyloxycarbonylamino-acetylamino)-benzoylamino]-pentanedioic acid di-tert-butyl ester

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Technology Process of (S)-2-[4-(2-Benzyloxycarbonylamino-acetylamino)-benzoylamino]-pentanedioic acid di-tert-butyl ester

There total 1 articles about (S)-2-[4-(2-Benzyloxycarbonylamino-acetylamino)-benzoylamino]-pentanedioic acid di-tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 78278-63-4
4-[(N-benzyloxycarbonyl-glycyl)-amino]-benzoic acid

: 32677-01-3
L-glutamic acid di-tert-butyl ester hydrochloride

: 162877-46-5
(S)-2-[4-(2-Benzyloxycarbonylamino-acetylamino)-benzoylamino]-pentanedioic acid di-tert-butyl ester

Guidance literature:: With triethylamine; diethyl dicarbonate; In N,N-dimethyl-formamide; for 1h; Ambient temperature;
DOI:10.1248/cpb.46.255

Reference yield: 94.0%

: 162877-46-5
(S)-2-[4-(2-Benzyloxycarbonylamino-acetylamino)-benzoylamino]-pentanedioic acid di-tert-butyl ester

: 162877-45-4
(S)-2-[4-(2-Amino-acetylamino)-benzoylamino]-pentanedioic acid di-tert-butyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1248/cpb.46.255

Reference yield:

: 162877-46-5
(S)-2-[4-(2-Benzyloxycarbonylamino-acetylamino)-benzoylamino]-pentanedioic acid di-tert-butyl ester

: 162878-15-1
(S)-2-(4-{2-[(R)-3-((R)-2,3-Bis-hexadecanoyloxy-propylsulfanyl)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-propionylamino]-acetylamino}-benzoylamino)-pentanedioic acid di-tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / H₂ / 10percent Pd/C / methanol

2: 56 percent / DEPC, Et₃N / dimethylformamide / 1 h / Ambient temperature

With hydrogen; triethylamine; diethyl dicarbonate; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1248/cpb.46.255