(2R,3R,3aR,4R,6R)-4-benzyloxy-2-[(1S)-1,2-dihydroxyethyl]-3-(dimethylphenylsilyl)-6-[(1S,2R)-(2-phenylcyclohexyl)oxy]hexahydroisoxazolo-[1,7b][1,2]oxazine

Base Information

Chemical Name:(2R,3R,3aR,4R,6R)-4-benzyloxy-2-[(1S)-1,2-dihydroxyethyl]-3-(dimethylphenylsilyl)-6-[(1S,2R)-(2-phenylcyclohexyl)oxy]hexahydroisoxazolo-[1,7b][1,2]oxazine
CAS No.:268202-13-7
Molecular Formula:C₃₅H₄₃NO₇Si
Molecular Weight:617.814
Hs Code.:

(2R,3R,3aR,4R,6R)-4-benzyloxy-2-[(1S)-1,2-dihydroxyethyl]-3-(dimethylphenylsilyl)-6-[(1S,2R)-(2-phenylcyclohexyl)oxy]hexahydroisoxazolo-[1,7b][1,2]oxazine

Synonyms:(2R,3R,3aR,4R,6R)-4-benzyloxy-2-[(1S)-1,2-dihydroxyethyl]-3-(dimethylphenylsilyl)-6-[(1S,2R)-(2-phenylcyclohexyl)oxy]hexahydroisoxazolo-[1,7b][1,2]oxazine

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Chemical Property of (2R,3R,3aR,4R,6R)-4-benzyloxy-2-[(1S)-1,2-dihydroxyethyl]-3-(dimethylphenylsilyl)-6-[(1S,2R)-(2-phenylcyclohexyl)oxy]hexahydroisoxazolo-[1,7b][1,2]oxazine

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Technology Process of (2R,3R,3aR,4R,6R)-4-benzyloxy-2-[(1S)-1,2-dihydroxyethyl]-3-(dimethylphenylsilyl)-6-[(1S,2R)-(2-phenylcyclohexyl)oxy]hexahydroisoxazolo-[1,7b][1,2]oxazine

There total 1 articles about (2R,3R,3aR,4R,6R)-4-benzyloxy-2-[(1S)-1,2-dihydroxyethyl]-3-(dimethylphenylsilyl)-6-[(1S,2R)-(2-phenylcyclohexyl)oxy]hexahydroisoxazolo-[1,7b][1,2]oxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: (2R,3R,3aR,4R,6R)-4-benzyloxy-2-{1-hydroxy-2-[dimethyl(1,1,2-trimethylpropyl)siloxy]ethyl}-3-(dimethylphenylsilyl)-6-[(1S,2R)-(2-phenylcyclohexyl)oxy]hexahydroisoxazolo-[1,7b][1,2]oxazine

: 268202-13-7
(2R,3R,3aR,4R,6R)-4-benzyloxy-2-[(1S)-1,2-dihydroxyethyl]-3-(dimethylphenylsilyl)-6-[(1S,2R)-(2-phenylcyclohexyl)oxy]hexahydroisoxazolo-[1,7b][1,2]oxazine

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 1h;
DOI:10.1021/jo991990d

Reference yield: 95.0%

: 4124-41-8
p-toluenesulfonylanhydride

: 268202-13-7
(2R,3R,3aR,4R,6R)-4-benzyloxy-2-[(1S)-1,2-dihydroxyethyl]-3-(dimethylphenylsilyl)-6-[(1S,2R)-(2-phenylcyclohexyl)oxy]hexahydroisoxazolo-[1,7b][1,2]oxazine

: 268202-17-1
Benzoic acid (2R,3R,3aR,4R,6R)-3-(dimethyl-phenyl-silanyl)-2-[(S)-1-hydroxy-2-(toluene-4-sulfonyloxy)-ethyl]-6-((1S,2R)-2-phenyl-cyclohexyloxy)-hexahydro-isoxazolo[2,3-b][1,2]oxazin-4-yl ester

Guidance literature:: With pyridine; at 20 ℃;
DOI:10.1021/jo991990d

Reference yield:

: 268202-13-7
(2R,3R,3aR,4R,6R)-4-benzyloxy-2-[(1S)-1,2-dihydroxyethyl]-3-(dimethylphenylsilyl)-6-[(1S,2R)-(2-phenylcyclohexyl)oxy]hexahydroisoxazolo-[1,7b][1,2]oxazine

: Benzoic acid (2R,3R,3aR,4R,6R)-3-(dimethyl-phenyl-silanyl)-2-((S)-2,2-dioxo-2λ⁶-[1,3,2]dioxathiolan-4-yl)-6-((1S,2R)-2-phenyl-cyclohexyloxy)-hexahydro-isoxazolo[2,3-b][1,2]oxazin-4-yl ester

Guidance literature:: (2R,3R,3aR,4R,6R)-4-benzyloxy-2-[(1S)-1,2-dihydroxyethyl]-3-(dimethylphenylsilyl)-6-[(1S,2R)-(2-phenylcyclohexyl)oxy]hexahydroisoxazolo-[1,7b][1,2]oxazine; With thionyl chloride;

With sodium periodate; ruthenium trichloride; Further stages.;
DOI:10.1021/jo991990d