(3S,4S,6R)-3-(tert-butyldimethylsilyloxy)-7-(tert-butyldiphenylsilyloxy)-4-(methoxymethoxy)-6-methylheptan-1-ol

Base Information

Chemical Name:(3S,4S,6R)-3-(tert-butyldimethylsilyloxy)-7-(tert-butyldiphenylsilyloxy)-4-(methoxymethoxy)-6-methylheptan-1-ol
CAS No.:1199807-65-2
Molecular Formula:C₃₂H₅₄O₅Si₂
Molecular Weight:574.949
Hs Code.:

Synonyms:(3S,4S,6R)-3-(tert-butyldimethylsilyloxy)-7-(tert-butyldiphenylsilyloxy)-4-(methoxymethoxy)-6-methylheptan-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,4S,6R)-3-(tert-butyldimethylsilyloxy)-7-(tert-butyldiphenylsilyloxy)-4-(methoxymethoxy)-6-methylheptan-1-ol

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Technology Process of (3S,4S,6R)-3-(tert-butyldimethylsilyloxy)-7-(tert-butyldiphenylsilyloxy)-4-(methoxymethoxy)-6-methylheptan-1-ol

There total 1 articles about (3S,4S,6R)-3-(tert-butyldimethylsilyloxy)-7-(tert-butyldiphenylsilyloxy)-4-(methoxymethoxy)-6-methylheptan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1199807-77-6
C₃₈H₆₈O₅Si₃

: 1199807-65-2
(3S,4S,6R)-3-(tert-butyldimethylsilyloxy)-7-(tert-butyldiphenylsilyloxy)-4-(methoxymethoxy)-6-methylheptan-1-ol

Guidance literature:: With methanol; toluene-4-sulfonic acid; at -10 ℃; for 0.25h; Inert atmosphere;
DOI:10.1021/ol9025183

Reference yield: 86.0%

: 1199807-65-2
(3S,4S,6R)-3-(tert-butyldimethylsilyloxy)-7-(tert-butyldiphenylsilyloxy)-4-(methoxymethoxy)-6-methylheptan-1-ol

: 1099-45-2
ethyl (triphenylphosphoranylidene)acetate

: 1199807-66-3
(5S,6S,8R,E)-ethyl 5-(tert-butyldimethylsilyloxy)-9-(tert-butyldiphenylsilyloxy)-6-(methoxymethoxy)-8-methylnon-2-enoate

Guidance literature:: In benzene; at 0 - 20 ℃; for 12h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ol9025183

Reference yield:

: 1199807-65-2
(3S,4S,6R)-3-(tert-butyldimethylsilyloxy)-7-(tert-butyldiphenylsilyloxy)-4-(methoxymethoxy)-6-methylheptan-1-ol

: C₃₂H₅₂O₅Si₂

Guidance literature:: With sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol9025183