methyl 5-amino>salicylate

Base Information

Chemical Name:methyl 5-amino>salicylate
CAS No.:152502-16-4
Molecular Formula:C₂₁H₂₂N₂O₈
Molecular Weight:430.414
Hs Code.:

methyl 5-<N-<methyl N-(benzyloxycarbonyl)-L-aspartyl ester>amino>salicylate

Synonyms:methyl 5-amino>salicylate

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Chemical Property of methyl 5-amino>salicylate

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Technology Process of methyl 5-amino>salicylate

There total 1 articles about methyl 5-amino>salicylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 3160-47-2
N-(benzyloxycarbonyl)-L-aspartic acid 4-methyl ester

: 42753-75-3
methyl 5-amino-2-hydroxybenzoate

: 152502-16-4
methyl 5-amino>salicylate

Guidance literature:: With 1H-imidazole; dicyclohexyl-carbodiimide; In ethyl acetate;
DOI:10.1021/jm00078a009

Reference yield: 91.0%

: 152502-16-4
methyl 5-amino>salicylate

: 152502-18-6
methyl 5-salicylate

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 6h; under 2585.7 Torr;
DOI:10.1021/jm00078a009

Reference yield:

: 152502-16-4
methyl 5-amino>salicylate

: 5-(N-L-aspartylamino)salicylic acid disodium salt

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / H₂ / 5percent Pd/C / methanol / 6 h / 2585.7 Torr

2: 94 percent / 1 N NaOH / 6 h / Ambient temperature

With sodium hydroxide; hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1021/jm00078a009