Benzoic acid (8S,8aR)-3-oxo-1,5,8,8a-tetrahydro-oxazolo[3,4-a]pyridin-8-yl ester

Base Information

Chemical Name:Benzoic acid (8S,8aR)-3-oxo-1,5,8,8a-tetrahydro-oxazolo[3,4-a]pyridin-8-yl ester
CAS No.:791608-16-7
Molecular Formula:C₁₄H₁₃NO₄
Molecular Weight:259.262
Hs Code.:

Synonyms:Benzoic acid (8S,8aR)-3-oxo-1,5,8,8a-tetrahydro-oxazolo[3,4-a]pyridin-8-yl ester

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Chemical Property of Benzoic acid (8S,8aR)-3-oxo-1,5,8,8a-tetrahydro-oxazolo[3,4-a]pyridin-8-yl ester

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Technology Process of Benzoic acid (8S,8aR)-3-oxo-1,5,8,8a-tetrahydro-oxazolo[3,4-a]pyridin-8-yl ester

There total 11 articles about Benzoic acid (8S,8aR)-3-oxo-1,5,8,8a-tetrahydro-oxazolo[3,4-a]pyridin-8-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 791608-14-5
Benzoic acid (S)-1-((R)-3-allyl-2-oxo-oxazolidin-4-yl)-allyl ester

: 791608-16-7
Benzoic acid (8S,8aR)-3-oxo-1,5,8,8a-tetrahydro-oxazolo[3,4-a]pyridin-8-yl ester

Guidance literature:: Grubbs catalyst first generation; In toluene; at 20 ℃;
DOI:10.1002/anie.200453863

Reference yield:

: 791607-96-0
(S)-1-[(R)-2-oxooxazolidin-4-yl]allyl benzoate

: 791608-16-7
Benzoic acid (8S,8aR)-3-oxo-1,5,8,8a-tetrahydro-oxazolo[3,4-a]pyridin-8-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / NaH / dimethylformamide / 0 - 20 °C

2: 99 percent / Grubbs catalyst / toluene / 20 °C

With sodium hydride; Grubbs catalyst first generation; In N,N-dimethyl-formamide; toluene;
DOI:10.1002/anie.200453863

Reference yield:

: 791607-94-8
[(2S,3S)-3-vinyloxiran-2-yl]methyl benzoylcarbamate

: 791608-16-7
Benzoic acid (8S,8aR)-3-oxo-1,5,8,8a-tetrahydro-oxazolo[3,4-a]pyridin-8-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / K₂CO₃; (C₈H₁₇)3CH₃NCl / CH₂Cl₂; H₂O / 20 °C

2: 81 percent / NaH / dimethylformamide / 0 - 20 °C

3: 99 percent / Grubbs catalyst / toluene / 20 °C

With (C₈H₁₇)3CH₃NCl; sodium hydride; potassium carbonate; Grubbs catalyst first generation; In dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1002/anie.200453863