10-(cyclohexylimino)-9-(ethoxymethyl)-7,9-diazaspiro[4.5]decane-6,8-dione

Base Information

Chemical Name:10-(cyclohexylimino)-9-(ethoxymethyl)-7,9-diazaspiro[4.5]decane-6,8-dione
CAS No.:1466431-60-6
Molecular Formula:C₁₇H₂₇N₃O₃
Molecular Weight:321.42
Hs Code.:

Synonyms:10-(cyclohexylimino)-9-(ethoxymethyl)-7,9-diazaspiro[4.5]decane-6,8-dione

Suppliers and Price of 10-(cyclohexylimino)-9-(ethoxymethyl)-7,9-diazaspiro[4.5]decane-6,8-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 10-(cyclohexylimino)-9-(ethoxymethyl)-7,9-diazaspiro[4.5]decane-6,8-dione

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 10-(cyclohexylimino)-9-(ethoxymethyl)-7,9-diazaspiro[4.5]decane-6,8-dione

There total 8 articles about 10-(cyclohexylimino)-9-(ethoxymethyl)-7,9-diazaspiro[4.5]decane-6,8-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1466431-57-1
10-(cyclohexylimino)-9-(ethoxymethyl)-7,9-diazaspiro[4.5]dec-2-ene-6,8-dione

: 1466431-60-6
10-(cyclohexylimino)-9-(ethoxymethyl)-7,9-diazaspiro[4.5]decane-6,8-dione

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethyl acetate; at 20 ℃; for 1h; under 1861.78 Torr;
DOI:10.1055/s-0033-1339179

Reference yield:

: 1466431-54-8
7-benzoyl-10-(cyclohexylimino)-9-(ethoxymethyl)-7,9-diazaspiro[4.5]dec-2-ene-6,8-dione

: 1466431-60-6
10-(cyclohexylimino)-9-(ethoxymethyl)-7,9-diazaspiro[4.5]decane-6,8-dione

Guidance literature:: Multi-step reaction with 2 steps

1: ammonia / dichloromethane; methanol / 1 h / 20 °C

2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 1 h / 20 °C / 1861.78 Torr

With palladium 10% on activated carbon; ammonia; hydrogen; In methanol; dichloromethane; ethyl acetate;
DOI:10.1055/s-0033-1339179

Reference yield:

: 1466431-50-4
5,5-diallyl-3-benzoyl-6-(cyclohexylimino)-1-(ethoxymethyl)dihydropyrimidine-2,4(1H,3H)-dione

: 1466431-60-6
10-(cyclohexylimino)-9-(ethoxymethyl)-7,9-diazaspiro[4.5]decane-6,8-dione

Guidance literature:: Multi-step reaction with 3 steps

1: Grubbs catalyst first generation / dichloromethane / 20 °C

2: ammonia / dichloromethane; methanol / 1 h / 20 °C

3: palladium 10% on activated carbon; hydrogen / ethyl acetate / 1 h / 20 °C / 1861.78 Torr

With Grubbs catalyst first generation; palladium 10% on activated carbon; ammonia; hydrogen; In methanol; dichloromethane; ethyl acetate;
DOI:10.1055/s-0033-1339179