4-amino-6-trifluoromethyl-benzene-1,3-disulfonic acid 1-amide 3-methylamide

Base Information

• Chemical Name: 4-amino-6-trifluoromethyl-benzene-1,3-disulfonic acid 1-amide 3-methylamide
• CAS No.: 735-25-1
• Molecular Formula: C₈H₁₀F₃N₃O₄S₂
• Molecular Weight: 333.312

Synonyms:4-amino-6-trifluoromethyl-benzene-1,3-disulfonic acid 1-amide 3-methylamide

Chemical Property of 4-amino-6-trifluoromethyl-benzene-1,3-disulfonic acid 1-amide 3-methylamide

Chemical Property:

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Technology Process of 4-amino-6-trifluoromethyl-benzene-1,3-disulfonic acid 1-amide 3-methylamide

There total 1 articles about 4-amino-6-trifluoromethyl-benzene-1,3-disulfonic acid 1-amide 3-methylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 4-amino-6-trifluoromethyl-benzene-1,3-disulfonic acid 1-amide 3-methylamide (735-25-1)

Guidance literature:

4-Amino-5-methylaminosulfonyl-2-trifluormethyl-benzolsulfochlorid u. konz. NH3;

Reference yield:

3-oxobutyraldehyde (625-34-3) + 4-amino-6-trifluoromethyl-benzene-1,3-disulfonic acid 1-amide 3-methylamide (735-25-1) → 2-methyl-1,1-dioxo-3-(2-oxo-propyl)-6-trifluoromethyl-1,2,3,4-tetrahydro-1λ6-benzo[1,2,4]thiadiazine-7-sulfonic acid amide (1457-14-3)

Guidance literature:

With hydrogenchloride; In N,N-dimethyl-formamide;

DOI:10.1021/jm00325a018

Reference yield:

4-amino-6-trifluoromethyl-benzene-1,3-disulfonic acid 1-amide 3-methylamide (735-25-1) + 3-Oxo-3-phenylpropanal (15397-33-8) → 2-methyl-1,1-dioxo-3-(2-oxo-2-phenyl-ethyl)-6-trifluoromethyl-1,2,3,4-tetrahydro-1λ6-benzo[1,2,4]thiadiazine-7-sulfonic acid amide (3754-13-0)

Guidance literature:

With hydrogenchloride; In N,N-dimethyl-formamide;

DOI:10.1021/jm00325a018

Downstream raw materials:

2-methyl-1,1-dioxo-3-(2-oxo-propyl)-6-trifluoromethyl-1,2,3,4-tetrahydro-1λ⁶-benzo[1,2,4]thiadiazine-7-sulfonic acid amide

N-(2-Hydroxy-cyclohexen-1-ylmethyliden)-5-trifluormethyl-2-methylsulfamoyl-4-sulfamoyl-anilin

2-methyl-1,1-dioxo-3-(2-oxo-2-phenyl-ethyl)-6-trifluoromethyl-1,2,3,4-tetrahydro-1λ⁶-benzo[1,2,4]thiadiazine-7-sulfonic acid amide

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