9-chloro-9-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-9,10-dihydro-9-stannaphenanthrene

Base Information

Chemical Name:9-chloro-9-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-9,10-dihydro-9-stannaphenanthrene
CAS No.:866367-23-9
Molecular Formula:C₄₀H₆₉ClSi₆Sn
Molecular Weight:872.664
Hs Code.:

Synonyms:9-chloro-9-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-9,10-dihydro-9-stannaphenanthrene

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Chemical Property of 9-chloro-9-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-9,10-dihydro-9-stannaphenanthrene

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Technology Process of 9-chloro-9-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-9,10-dihydro-9-stannaphenanthrene

There total 4 articles about 9-chloro-9-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-9,10-dihydro-9-stannaphenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 866367-30-8
(((CH₃)3Si)2CH)3C₆H₂SnCl₂C₆H₄C₆H₄CH₂Br

: 866367-23-9
9-chloro-9-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-9,10-dihydro-9-stannaphenanthrene

Guidance literature:: With Mg; LiAlH₄; In tetrachloromethane; 1. Mg, 2. LiH4, 3. CCl4;
DOI:10.1246/cl.2005.1088

Reference yield:

: 251320-87-3
2-bromo-2'-methylbiphenyl

: 866367-23-9
9-chloro-9-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-9,10-dihydro-9-stannaphenanthrene

Guidance literature:: Multi-step reaction with 3 steps

1: n-BuLi; LiAlH₄ / tetrachloromethane

3: Mg; LiAlH₄ / tetrachloromethane

With n-BuLi; LiAlH₄; Mg; In tetrachloromethane;
DOI:10.1246/cl.2005.1088

Reference yield:

: 135139-65-0
2,4,6-tris[bis(trimethylsilyl)methyl]phenyl-trichloro stannane

: 866367-23-9
9-chloro-9-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-9,10-dihydro-9-stannaphenanthrene

Guidance literature:: Multi-step reaction with 3 steps

1: n-BuLi; LiAlH₄ / tetrachloromethane

3: Mg; LiAlH₄ / tetrachloromethane

With n-BuLi; LiAlH₄; Mg; In tetrachloromethane;
DOI:10.1246/cl.2005.1088