(4-tert-butyl-phenyl)-(5-{(4-tert-butyl-phenyl)-[5-(hydroxy-{4-[(triisopropylsilanyl)-ethynyl]-phenyl}-methyl)-1H-pyrrol-2-yl]-methyl}-1H-pyrrol-2-yl)-methanol

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Chemical Name:(4-tert-butyl-phenyl)-(5-{(4-tert-butyl-phenyl)-[5-(hydroxy-{4-[(triisopropylsilanyl)-ethynyl]-phenyl}-methyl)-1H-pyrrol-2-yl]-methyl}-1H-pyrrol-2-yl)-methanol
CAS No.:1026729-83-8
Molecular Formula:C₄₈H₆₂N₂O₂Si
Molecular Weight:727.118
Hs Code.:

(4-<i>tert</i>-butyl-phenyl)-(5-{(4-<i>tert</i>-butyl-phenyl)-[5-(hydroxy-{4-[(triisopropylsilanyl)-ethynyl]-phenyl}-methyl)-1<i>H</i>-pyrrol-2-yl]-methyl}-1<i>H</i>-pyrrol-2-yl)-methanol

Synonyms:(4-tert-butyl-phenyl)-(5-{(4-tert-butyl-phenyl)-[5-(hydroxy-{4-[(triisopropylsilanyl)-ethynyl]-phenyl}-methyl)-1H-pyrrol-2-yl]-methyl}-1H-pyrrol-2-yl)-methanol

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Chemical Property of (4-tert-butyl-phenyl)-(5-{(4-tert-butyl-phenyl)-[5-(hydroxy-{4-[(triisopropylsilanyl)-ethynyl]-phenyl}-methyl)-1H-pyrrol-2-yl]-methyl}-1H-pyrrol-2-yl)-methanol

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Technology Process of (4-tert-butyl-phenyl)-(5-{(4-tert-butyl-phenyl)-[5-(hydroxy-{4-[(triisopropylsilanyl)-ethynyl]-phenyl}-methyl)-1H-pyrrol-2-yl]-methyl}-1H-pyrrol-2-yl)-methanol

There total 10 articles about (4-tert-butyl-phenyl)-(5-{(4-tert-butyl-phenyl)-[5-(hydroxy-{4-[(triisopropylsilanyl)-ethynyl]-phenyl}-methyl)-1H-pyrrol-2-yl]-methyl}-1H-pyrrol-2-yl)-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 307931-02-8
1-(4-tert-butylbenzoyl)-5-(4-tert-butylphenyl)-9-{4-[2-(triisopropylsilyl)ethynyl]benzoyl}dipyrromethane

: 1026729-83-8
(4-tert-butyl-phenyl)-(5-{(4-tert-butyl-phenyl)-[5-(hydroxy-{4-[(triisopropylsilanyl)-ethynyl]-phenyl}-methyl)-1H-pyrrol-2-yl]-methyl}-1H-pyrrol-2-yl)-methanol

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; methanol; at 20 ℃; for 0.666667h;
DOI:10.1021/jo000882k

Reference yield:

: 51934-41-9
4-iodobenzoic acid ethyl ester

: 1026729-83-8
(4-tert-butyl-phenyl)-(5-{(4-tert-butyl-phenyl)-[5-(hydroxy-{4-[(triisopropylsilanyl)-ethynyl]-phenyl}-methyl)-1H-pyrrol-2-yl]-methyl}-1H-pyrrol-2-yl)-methanol

Guidance literature:: Multi-step reaction with 5 steps

1.1: CuI; Et₃N / Pd(PPh₃)2Cl₂ / 13 h / 20 - 50 °C

2.1: 12.15 g / NaOH / ethanol; H₂O / 12 h / 20 °C

3.1: 85 percent / SOCl₂ / benzene / 36 h / Heating

4.1: EtMgBr / toluene; tetrahydrofuran / 0.08 h / 20 °C

4.2: 67 percent / toluene / 20 °C

5.1: NaBH₄ / tetrahydrofuran; methanol / 0.67 h / 20 °C

With sodium hydroxide; sodium tetrahydroborate; copper(l) iodide; thionyl chloride; ethylmagnesium bromide; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; methanol; ethanol; water; toluene; benzene; 1.1: coupling / 2.1: Hydrolysis / 3.1: Substitution / 4.1: Metallation / 4.2: Acylation / 5.1: Reduction;
DOI:10.1021/jo000882k

Reference yield:

: 89343-06-6
tris-iso-propylsilyl acetylene

: 1026729-83-8
(4-tert-butyl-phenyl)-(5-{(4-tert-butyl-phenyl)-[5-(hydroxy-{4-[(triisopropylsilanyl)-ethynyl]-phenyl}-methyl)-1H-pyrrol-2-yl]-methyl}-1H-pyrrol-2-yl)-methanol

Guidance literature:: Multi-step reaction with 5 steps

1.1: CuI; Et₃N / Pd(PPh₃)2Cl₂ / 13 h / 20 - 50 °C

2.1: 12.15 g / NaOH / ethanol; H₂O / 12 h / 20 °C

3.1: 85 percent / SOCl₂ / benzene / 36 h / Heating

4.1: EtMgBr / toluene; tetrahydrofuran / 0.08 h / 20 °C

4.2: 67 percent / toluene / 20 °C

5.1: NaBH₄ / tetrahydrofuran; methanol / 0.67 h / 20 °C

With sodium hydroxide; sodium tetrahydroborate; copper(l) iodide; thionyl chloride; ethylmagnesium bromide; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; methanol; ethanol; water; toluene; benzene; 1.1: coupling / 2.1: Hydrolysis / 3.1: Substitution / 4.1: Metallation / 4.2: Acylation / 5.1: Reduction;
DOI:10.1021/jo000882k