Methyl-2,3,4-tri-O-acetyl-beta-D-xylopyranoside

Base Information

Chemical Name:Methyl-2,3,4-tri-O-acetyl-beta-D-xylopyranoside
CAS No.:13007-37-9
Molecular Formula:C₁₂H₁₈O₈
Molecular Weight:290.27
Hs Code.:
DSSTox Substance ID:DTXSID701256354
Nikkaji Number:J610.356A
Mol file:13007-37-9.mol

Synonyms:13007-37-9;METHYL-2,3,4-TRI-O-ACETYL-BETA-D-XYLOPYRANOSIDE;[(3R,4S,5R,6R)-4,5-diacetyloxy-6-methoxyoxan-3-yl] acetate;(3R,4S,5R,6R)-4,5-bis(acetyloxy)-6-methoxyoxan-3-yl acetate;2,3,4-tri-O-Ac;SCHEMBL7151845;YBESHGJFPWHRBW-WRWGMCAJSA-N;DTXSID701256354;.beta.-D-Xylopyranoside, methyl, triacetate;Xylopyranoside, methyl, triacetate, .beta.-D-;Methyl 2,3,4-tri-O-acetyl-beta-D-xylopyranoside

Suppliers and Price of Methyl-2,3,4-tri-O-acetyl-beta-D-xylopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
METHYL-2,3,4-TRI-O-ACETYL-BETA-D-XYLOPYRANOSIDE 95.00%
5MG
$ 501.74

Total 6 raw suppliers

Chemical Property of Methyl-2,3,4-tri-O-acetyl-beta-D-xylopyranoside

Chemical Property:

Melting Point:115 °C(Solv: water (7732-18-5))
Boiling Point:332.1±42.0 °C(Predicted)
PSA：97.36000
Density:1.24±0.1 g/cm3(Predicted)
LogP:-0.21580
XLogP3:-0.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:8
Rotatable Bond Count:7
Exact Mass:290.10016753
Heavy Atom Count:20
Complexity:380

Purity/Quality:

95% ^*data from raw suppliers

METHYL-2,3,4-TRI-O-ACETYL-BETA-D-XYLOPYRANOSIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)OC1COC(C(C1OC(=O)C)OC(=O)C)OC
Isomeric SMILES:CC(=O)O[C@@H]1CO[C@H]([C@@H]([C@H]1OC(=O)C)OC(=O)C)OC

Technology Process of Methyl-2,3,4-tri-O-acetyl-beta-D-xylopyranoside

There total 11 articles about Methyl-2,3,4-tri-O-acetyl-beta-D-xylopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 108-24-7
acetic anhydride

: 612-05-5
methyl-β-D-xylopyranoside

: 13007-37-9,14200-56-7,14520-32-2,20880-54-0,21615-78-1,32445-37-7,32445-38-8,32453-56-8,32453-57-9,32453-58-0,32453-59-1,41897-43-2,41897-44-3,57568-88-4,57568-89-5,63097-04-1,86717-28-4,91877-72-4,100428-04-4
methyl 2,3,4-tri-O-acetyl-β-D-xylopyranoside

Guidance literature:: With pyridine;
DOI:10.1016/S0008-6215(97)00104-3

Reference yield:

: 95851-48-2,121430-13-5
C₄₂H₆₈O₁₂

: 13007-37-9,14200-56-7,14520-32-2,20880-54-0,21615-78-1,32445-37-7,32445-38-8,32453-56-8,32453-57-9,32453-58-0,32453-59-1,41897-43-2,41897-44-3,57568-88-4,57568-89-5,63097-04-1,86717-28-4,91877-72-4,100428-04-4
peracetate of methyl L-arabinos1de

Guidance literature:: Multi-step reaction with 2 steps

1: 2 N HCl / methanol / 3 h / Heating

2: pyridine / Ambient temperature

With pyridine; hydrogenchloride; In methanol;
DOI:10.1248/cpb.33.1