(S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-((R)-3-(allyloxy)-2-((4-nitrobenzyloxy)carbonylamino)-3-oxopropoxy)propanoic acid

Base Information

• Chemical Name: (S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-((R)-3-(allyloxy)-2-((4-nitrobenzyloxy)carbonylamino)-3-oxopropoxy)propanoic acid
• CAS No.: 1200571-45-4
• Molecular Formula: C₃₂H₃₁N₃O₁₁
• Molecular Weight: 633.612

Synonyms:(S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-((R)-3-(allyloxy)-2-((4-nitrobenzyloxy)carbonylamino)-3-oxopropoxy)propanoic acid

Chemical Property of (S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-((R)-3-(allyloxy)-2-((4-nitrobenzyloxy)carbonylamino)-3-oxopropoxy)propanoic acid

Chemical Property:

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Technology Process of (S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-((R)-3-(allyloxy)-2-((4-nitrobenzyloxy)carbonylamino)-3-oxopropoxy)propanoic acid

There total 1 articles about (S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-((R)-3-(allyloxy)-2-((4-nitrobenzyloxy)carbonylamino)-3-oxopropoxy)propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(R)-allyl 3-((S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-tert-butoxy-3-oxopropoxy)-2-((4-nitrobenzyloxy)carbonylamino)propanoate → (S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-((R)-3-(allyloxy)-2-((4-nitrobenzyloxy)carbonylamino)-3-oxopropoxy)propanoic acid (1200571-45-4)

Guidance literature:

With phenylsilane; trifluoroacetic acid; In dichloromethane; at 25 ℃; for 2h;

DOI:10.1021/ol9025205

Reference yield:

(S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-((R)-3-(allyloxy)-2-((4-nitrobenzyloxy)carbonylamino)-3-oxopropoxy)propanoic acid (1200571-45-4) + C61H98N13O18PolS → C93H127N16O28PolS

Guidance literature:

(S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-3-((R)-3-(allyloxy)-2-((4-nitrobenzyloxy)carbonylamino)-3-oxopropoxy)propanoic acid; With 4-methyl-morpholine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; In N,N-dimethyl-formamide; for 0.0833333h;

C₆₁H₉₈N₁₃O₁₈PolS; In N,N-dimethyl-formamide; for 2h; solid phase reaction;

DOI:10.1021/ol9025205

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