N,N-bis{(E)-4-[2-(dithieno[2,3-b:3',2'-d]thiophen-2-yl)vinyl]phenyl}-N-phenylamine

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Chemical Name:N,N-bis{(E)-4-[2-(dithieno[2,3-b:3',2'-d]thiophen-2-yl)vinyl]phenyl}-N-phenylamine
CAS No.:1610617-72-5
Molecular Formula:C₃₈H₂₃NS₆
Molecular Weight:686.003
Hs Code.:

Synonyms:N,N-bis{(E)-4-[2-(dithieno[2,3-b:3',2'-d]thiophen-2-yl)vinyl]phenyl}-N-phenylamine

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Chemical Property of N,N-bis{(E)-4-[2-(dithieno[2,3-b:3',2'-d]thiophen-2-yl)vinyl]phenyl}-N-phenylamine

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Technology Process of N,N-bis{(E)-4-[2-(dithieno[2,3-b:3',2'-d]thiophen-2-yl)vinyl]phenyl}-N-phenylamine

There total 4 articles about N,N-bis{(E)-4-[2-(dithieno[2,3-b:3',2'-d]thiophen-2-yl)vinyl]phenyl}-N-phenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: N,N-di{4-[(triphenylphosphoniumyl)methyl]phenyl}phenylamine dibromide

: 1059629-16-1
dithieno[2,3-b:3',2'-d]thiophene-2-carbaldehyde

: 1610617-72-5
N,N-bis{(E)-4-[2-(dithieno[2,3-b:3',2'-d]thiophen-2-yl)vinyl]phenyl}-N-phenylamine

Guidance literature:: N,N-di{4-[(triphenylphosphoniumyl)methyl]phenyl}phenylamine dibromide; dithieno[2,3-b:3',2'-d]thiophene-2-carbaldehyde; With potassium tert-butylate; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere; Schlenk technique;

With iodine; In tetrahydrofuran; for 6h; Inert atmosphere; Schlenk technique; Reflux;
DOI:10.1016/j.tet.2014.04.031

Reference yield:

: ((phenylazanediyl)bis(4,1-phenylene))dimethanol

: 1610617-72-5
N,N-bis{(E)-4-[2-(dithieno[2,3-b:3',2'-d]thiophen-2-yl)vinyl]phenyl}-N-phenylamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: chloroform / 2 h / Inert atmosphere; Schlenk technique; Reflux

2.1: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere; Schlenk technique

2.2: 6 h / Inert atmosphere; Schlenk technique; Reflux

With potassium tert-butylate; In tetrahydrofuran; chloroform; 2.1: |Wittig Olefination;
DOI:10.1016/j.tet.2014.04.031

Reference yield:

: 603-34-9
N,N-diphenylaminobenzene

: 1610617-72-5
N,N-bis{(E)-4-[2-(dithieno[2,3-b:3',2'-d]thiophen-2-yl)vinyl]phenyl}-N-phenylamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: trichlorophosphate / 48 h / 80 - 90 °C / Inert atmosphere; Schlenk technique

2.1: sodium tetrahydroborate / dichloromethane / 2 h / 20 °C / Inert atmosphere; Schlenk technique

3.1: chloroform / 2 h / Inert atmosphere; Schlenk technique; Reflux

4.1: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere; Schlenk technique

4.2: 6 h / Inert atmosphere; Schlenk technique; Reflux

With sodium tetrahydroborate; potassium tert-butylate; trichlorophosphate; In tetrahydrofuran; dichloromethane; chloroform; 4.1: |Wittig Olefination;
DOI:10.1016/j.tet.2014.04.031