2,5-bis(5-benzyloxycarbonyl-3-ethyl-4-methyl-2-pyrrolylmethyl)-3,4-diphenylpyrrole

Base Information

Chemical Name:2,5-bis(5-benzyloxycarbonyl-3-ethyl-4-methyl-2-pyrrolylmethyl)-3,4-diphenylpyrrole
CAS No.:444108-82-1
Molecular Formula:C₄₈H₄₇N₃O₄
Molecular Weight:729.919
Hs Code.:

Synonyms:2,5-bis(5-benzyloxycarbonyl-3-ethyl-4-methyl-2-pyrrolylmethyl)-3,4-diphenylpyrrole

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Chemical Property of 2,5-bis(5-benzyloxycarbonyl-3-ethyl-4-methyl-2-pyrrolylmethyl)-3,4-diphenylpyrrole

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Technology Process of 2,5-bis(5-benzyloxycarbonyl-3-ethyl-4-methyl-2-pyrrolylmethyl)-3,4-diphenylpyrrole

There total 1 articles about 2,5-bis(5-benzyloxycarbonyl-3-ethyl-4-methyl-2-pyrrolylmethyl)-3,4-diphenylpyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1632-48-0
3,4-diphenyl-1H-pyrrole

: 3750-36-5
benzyl 5-(acetoxymethyl)-4-ethyl-3-methyl-1H-pyrrole-2-carboxylate

: 444108-82-1
2,5-bis(5-benzyloxycarbonyl-3-ethyl-4-methyl-2-pyrrolylmethyl)-3,4-diphenylpyrrole

Guidance literature:: In ethanol; acetic acid; for 16h; Heating;
DOI:10.1021/jo020267b

Reference yield:

: 444108-82-1
2,5-bis(5-benzyloxycarbonyl-3-ethyl-4-methyl-2-pyrrolylmethyl)-3,4-diphenylpyrrole

: 444108-83-2
C₃₄H₃₅N₃O₄

Guidance literature:: With hydrogen; triethylamine; 10percent Pd/C; In tetrahydrofuran; methanol; under 2068.65 Torr;
DOI:10.1021/jo020267b

Reference yield:

: 444108-82-1
2,5-bis(5-benzyloxycarbonyl-3-ethyl-4-methyl-2-pyrrolylmethyl)-3,4-diphenylpyrrole

: 8,17-diethyl-7,18-dimethyl-12,13-diphenylbenzo[b]-21-carbaporphyrin

Guidance literature:: Multi-step reaction with 2 steps

1.1: Et₃N; H₂ / 10percent Pd/C / tetrahydrofuran; methanol / 2068.65 Torr

2.1: TFA / CH₂Cl₂ / 2 h

2.2: 53 mg / DDQ / CH₂Cl₂ / 1 h

With hydrogen; triethylamine; trifluoroacetic acid; 10percent Pd/C; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jo020267b