dimethyl (1'R,2'S,3'R,4'R)-3-(1',2',3',4',5'-pentahydroxypentyl)-4-phenyl-1H-pyrrole-2,5-dicabroxylate

Base Information

Chemical Name:dimethyl (1'R,2'S,3'R,4'R)-3-(1',2',3',4',5'-pentahydroxypentyl)-4-phenyl-1H-pyrrole-2,5-dicabroxylate
CAS No.:935694-00-1
Molecular Formula:C₁₉H₂₃NO₉
Molecular Weight:409.393
Hs Code.:

Synonyms:dimethyl (1'R,2'S,3'R,4'R)-3-(1',2',3',4',5'-pentahydroxypentyl)-4-phenyl-1H-pyrrole-2,5-dicabroxylate

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Chemical Property of dimethyl (1'R,2'S,3'R,4'R)-3-(1',2',3',4',5'-pentahydroxypentyl)-4-phenyl-1H-pyrrole-2,5-dicabroxylate

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Technology Process of dimethyl (1'R,2'S,3'R,4'R)-3-(1',2',3',4',5'-pentahydroxypentyl)-4-phenyl-1H-pyrrole-2,5-dicabroxylate

There total 4 articles about dimethyl (1'R,2'S,3'R,4'R)-3-(1',2',3',4',5'-pentahydroxypentyl)-4-phenyl-1H-pyrrole-2,5-dicabroxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 935693-90-6
dimethyl (1'R,2'S,3'R,4'R)-4-(1',2',3',4',5'-pentabenzoxypentyl)-5-phenylpyridazine-3,6-dicarboxylate

: 935694-00-1
dimethyl (1'R,2'S,3'R,4'R)-3-(1',2',3',4',5'-pentahydroxypentyl)-4-phenyl-1H-pyrrole-2,5-dicabroxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 46 percent / zinc / acetic acid / 0.5 h / Heating

2: 89 percent / H₂ / Pd/C / methanol / 1 h / 20 °C

With hydrogen; zinc; palladium on activated charcoal; In methanol; acetic acid;
DOI:10.1002/ejoc.200700102

Reference yield:

: 2166-14-5
1,2,4,5-tetrazine-3,6-dicarboxylic acid dimethyl ester

: 935694-00-1
dimethyl (1'R,2'S,3'R,4'R)-3-(1',2',3',4',5'-pentahydroxypentyl)-4-phenyl-1H-pyrrole-2,5-dicabroxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 55 percent / toluene / 120 h / Heating

2: 46 percent / zinc / acetic acid / 0.5 h / Heating

3: 89 percent / H₂ / Pd/C / methanol / 1 h / 20 °C

With hydrogen; zinc; palladium on activated charcoal; In methanol; acetic acid; toluene;
DOI:10.1002/ejoc.200700102

Reference yield:

: 935693-85-9
(2R,3R,4S,5R)-1,3,4-tribenzoxy-7-phenylhept-6-yne-2,5-diol

: 935694-00-1
dimethyl (1'R,2'S,3'R,4'R)-3-(1',2',3',4',5'-pentahydroxypentyl)-4-phenyl-1H-pyrrole-2,5-dicabroxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / sodium hydride / tetrahydrofuran; dimethylformamide / 20 °C

2: 55 percent / toluene / 120 h / Heating

3: 5 percent / zinc / acetic acid / 15 h / Heating

4: 89 percent / H₂ / Pd/C / methanol / 1 h / 20 °C

With hydrogen; sodium hydride; zinc; palladium on activated charcoal; In tetrahydrofuran; methanol; acetic acid; N,N-dimethyl-formamide; toluene;
DOI:10.1002/ejoc.200700102