Technology Process of 1-morpholino-1,9-octadecadiene
There total 1 articles about 1-morpholino-1,9-octadecadiene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
toluene-4-sulfonic acid;
In
benzene;
for 20h;
Heating;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) 9-BBN / 1.) THF, 25 deg C, 3 h, 2.) methanol, reflux, 2 h
2: 1.) 9-BBN, 2.) lithium diisopropylamide, 3.) NaOH, H2O2
3: diethyl ether
With
sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; dihydrogen peroxide; lithium diisopropyl amide;
In
diethyl ether;
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 1.) 9-BBN / 1.) THF, 25 deg C, 3 h, 2.) methanol, reflux, 2 h
2: 1.) 9-BBN, 2.) lithium diisopropylamide, 3.) NaOH, H2O2
3: diethyl ether
4: 70 percent / LAH / diethyl ether / 5 h
5: 91 percent / pyridinium chlorochromate / CH2Cl2 / 1 h
6: 85 percent / diethyl ether / 5 h / Heating
7: 96 percent / pyridine / 24 h / Heating
8: 95 percent / LAH / diethyl ether
With
pyridine; sodium hydroxide; lithium aluminium tetrahydride; 9-borabicyclo[3.3.1]nonane dimer; dihydrogen peroxide; pyridinium chlorochromate; lithium diisopropyl amide;
In
diethyl ether; dichloromethane;