Technology Process of meerwein reagent
There total 8 articles about meerwein reagent which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-chloro-succinimide; triethylamine;
In
chloroform;
at 0 ℃;
DOI:10.1002/anie.201006528
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydroxylamine hydrochloride; potassium carbonate / methanol; water / 1 h / 0 °C
2: N-chloro-succinimide; triethylamine / chloroform / 0 °C
With
N-chloro-succinimide; hydroxylamine hydrochloride; potassium carbonate; triethylamine;
In
methanol; chloroform; water;
DOI:10.1002/anie.201006528
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione / chloroform / 0 - 20 °C
2.1: tetra-N-butylammonium tribromide; orthoformic acid triethyl ester / 0 - 20 °C
3.1: n-butyllithium / tetrahydrofuran; diethyl ether; hexane / -78 °C / Inert atmosphere
3.2: -78 - 0 °C / Inert atmosphere
4.1: hydroxylamine hydrochloride; potassium carbonate / methanol; water / 1 h / 0 °C
5.1: N-chloro-succinimide; triethylamine / chloroform / 0 °C
With
N-chloro-succinimide; n-butyllithium; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; hydroxylamine hydrochloride; tetra-N-butylammonium tribromide; potassium carbonate; triethylamine; orthoformic acid triethyl ester;
In
tetrahydrofuran; methanol; diethyl ether; hexane; chloroform; water;
DOI:10.1002/anie.201006528
