C₁₄H₂₂OSi

Base Information

Chemical Name:C₁₄H₂₂OSi
CAS No.:1378249-57-0
Molecular Formula:C₁₄H₂₂OSi
Molecular Weight:234.414
Hs Code.:

Synonyms:C₁₄H₂₂OSi

Suppliers and Price of C₁₄H₂₂OSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₂₂OSi

Chemical Property:

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Technology Process of C₁₄H₂₂OSi

There total 4 articles about C₁₄H₂₂OSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₃₀O₂Si

: 1378249-57-0
C₁₄H₂₂OSi

Guidance literature:: With toluene-4-sulfonic acid; In methanol; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1021/ja302520h

Reference yield:

: 1378249-55-8
C₁₄H₂₆O₂Si

: 1378249-57-0
C₁₄H₂₂OSi

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / methanol / 1 h / 20 °C / Inert atmosphere

2.1: n-butyllithium / 0.5 h / -78 °C / Inert atmosphere

2.2: 3 h / -78 - 20 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / diethyl ether / 22 h / 0 - 20 °C / Inert atmosphere

3.2: Inert atmosphere

4.1: toluene-4-sulfonic acid / methanol / 6 h / 20 °C / Inert atmosphere

With n-butyllithium; diisobutylaluminium hydride; potassium carbonate; toluene-4-sulfonic acid; In methanol; diethyl ether;
DOI:10.1021/ja302520h

Reference yield:

: C₁₁H₁₈O₂

: 1378249-57-0
C₁₄H₂₂OSi

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / 0.5 h / -78 °C / Inert atmosphere

1.2: 3 h / -78 - 20 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / diethyl ether / 22 h / 0 - 20 °C / Inert atmosphere

2.2: Inert atmosphere

3.1: toluene-4-sulfonic acid / methanol / 6 h / 20 °C / Inert atmosphere

With n-butyllithium; diisobutylaluminium hydride; toluene-4-sulfonic acid; In methanol; diethyl ether;
DOI:10.1021/ja302520h