C₁₈H₁₂BrN

Base Information

Chemical Name:C₁₈H₁₂BrN
CAS No.:1428635-28-2
Molecular Formula:C₁₈H₁₂BrN
Molecular Weight:322.204
Hs Code.:

Synonyms:C₁₈H₁₂BrN

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Chemical Property of C₁₈H₁₂BrN

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Technology Process of C₁₈H₁₂BrN

There total 5 articles about C₁₈H₁₂BrN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: C₁₈H₁₂BrNO₂

: 1428635-28-2
C₁₈H₁₂BrN

Guidance literature:: With triethyl phosphate; In 1,2-dichloro-benzene; at 150 ℃; for 12h;

Reference yield:

: 98-80-6
phenylboronic acid

: 1428635-28-2
C₁₈H₁₂BrN

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / toluene; ethanol; water / 2 h / 90 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

2.2: 2 h

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / toluene; ethanol; water / 2 h / 90 °C

4.1: triethyl phosphate / 1,2-dichloro-benzene / 12 h / 150 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; triethyl phosphate; potassium carbonate; In tetrahydrofuran; ethanol; hexane; water; 1,2-dichloro-benzene; toluene;

Reference yield:

: C₁₂H₁₂B₂O₄

: 1428635-28-2
C₁₈H₁₂BrN

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / toluene; ethanol; water / 2 h / 90 °C

2: triethyl phosphate / 1,2-dichloro-benzene / 12 h / 150 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethyl phosphate; potassium carbonate; In ethanol; water; 1,2-dichloro-benzene; toluene;