2-butyl-7-methoxycarbonyl-4-{4-[(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)methyl]cyclohexanecarboxamido}-1-(2-hydroxy-2-methylpropyl)-1H-imidazo[4,5-c]quinoline

Base Information

Chemical Name:2-butyl-7-methoxycarbonyl-4-{4-[(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)methyl]cyclohexanecarboxamido}-1-(2-hydroxy-2-methylpropyl)-1H-imidazo[4,5-c]quinoline
CAS No.:1426395-64-3
Molecular Formula:C₃₂H₃₉N₅O₆
Molecular Weight:589.692
Hs Code.:

2-butyl-7-methoxycarbonyl-4-{4-[(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)methyl]cyclohexanecarboxamido}-1-(2-hydroxy-2-methylpropyl)-1H-imidazo[4,5-c]quinoline

Synonyms:2-butyl-7-methoxycarbonyl-4-{4-[(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)methyl]cyclohexanecarboxamido}-1-(2-hydroxy-2-methylpropyl)-1H-imidazo[4,5-c]quinoline

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Chemical Property of 2-butyl-7-methoxycarbonyl-4-{4-[(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)methyl]cyclohexanecarboxamido}-1-(2-hydroxy-2-methylpropyl)-1H-imidazo[4,5-c]quinoline

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Technology Process of 2-butyl-7-methoxycarbonyl-4-{4-[(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)methyl]cyclohexanecarboxamido}-1-(2-hydroxy-2-methylpropyl)-1H-imidazo[4,5-c]quinoline

There total 5 articles about 2-butyl-7-methoxycarbonyl-4-{4-[(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)methyl]cyclohexanecarboxamido}-1-(2-hydroxy-2-methylpropyl)-1H-imidazo[4,5-c]quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 64987-85-5
4-(N-maleimidomethyl)cyclohexane-1-carboxylic acid N-succinimidyl ester

: 1375262-88-6
4-amino-2-butyl-1-(2-hydroxyl-2-methylpropyl)-7-methoxycarbonyl-1H-imidazo[4,5-c]quinoline

: 1426395-64-3
2-butyl-7-methoxycarbonyl-4-{4-[(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)methyl]cyclohexanecarboxamido}-1-(2-hydroxy-2-methylpropyl)-1H-imidazo[4,5-c]quinoline

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 50 ℃; for 24h;

Reference yield:

: 919-29-9
triethyl orthovalerate

: 1426395-64-3
2-butyl-7-methoxycarbonyl-4-{4-[(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)methyl]cyclohexanecarboxamido}-1-(2-hydroxy-2-methylpropyl)-1H-imidazo[4,5-c]quinoline

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / tetrahydrofuran / 5 h / Reflux

1.2: 15 h / 25 °C

2.1: diiodomethane; isopentyl nitrite / chloroform / 0.83 h / 80 °C

3.1: palladium diacetate; triphenylphosphine; sodium carbonate / 1,2-dimethoxyethane; water / 21 h / 100 °C

4.1: hydrogenchloride / 1,4-dioxane / 15 h / Reflux

5.1: triethylamine / N,N-dimethyl-formamide / 24 h / 50 °C

With hydrogenchloride; diiodomethane; palladium diacetate; sodium carbonate; triethylamine; triphenylphosphine; isopentyl nitrite; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; chloroform; water; N,N-dimethyl-formamide;

Reference yield:

: 1375262-90-0
5-amino-2-butyl-1-(2-hydroxy-2-methylpropyl)-1H-imidazole-4-carbonitrile

: 1426395-64-3
2-butyl-7-methoxycarbonyl-4-{4-[(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)methyl]cyclohexanecarboxamido}-1-(2-hydroxy-2-methylpropyl)-1H-imidazo[4,5-c]quinoline

Guidance literature:: Multi-step reaction with 4 steps

1: diiodomethane; isopentyl nitrite / chloroform / 0.83 h / 80 °C

2: palladium diacetate; triphenylphosphine; sodium carbonate / 1,2-dimethoxyethane; water / 21 h / 100 °C

3: hydrogenchloride / 1,4-dioxane / 15 h / Reflux

4: triethylamine / N,N-dimethyl-formamide / 24 h / 50 °C

With hydrogenchloride; diiodomethane; palladium diacetate; sodium carbonate; triethylamine; triphenylphosphine; isopentyl nitrite; In 1,4-dioxane; 1,2-dimethoxyethane; chloroform; water; N,N-dimethyl-formamide;