C₄₄H₅₈N₁₀O₁₃

Base Information

Chemical Name:C₄₄H₅₈N₁₀O₁₃
CAS No.:1469300-13-7
Molecular Formula:C₄₄H₅₈N₁₀O₁₃
Molecular Weight:935.004
Hs Code.:

C<sub>44</sub>H<sub>58</sub>N<sub>10</sub>O<sub>13</sub>

Synonyms:C₄₄H₅₈N₁₀O₁₃

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Chemical Property of C₄₄H₅₈N₁₀O₁₃

Chemical Property:

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Technology Process of C₄₄H₅₈N₁₀O₁₃

There total 12 articles about C₄₄H₅₈N₁₀O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1469300-22-8
C₂₀H₂₇N₅O₆

: 1469300-23-9
C₂₄H₃₃N₅O₈

: 1469300-13-7
C₄₄H₅₈N₁₀O₁₃

Guidance literature:: C₂₄H₃₃N₅O₈; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 ℃; for 0.166667h; Inert atmosphere;

C₂₀H₂₇N₅O₆; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1002/anie.201304239

Reference yield:

: C₁₃H₁₇N₃O₃

: 1469300-13-7
C₄₄H₅₈N₁₀O₁₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: boron trifluoride diethyl etherate / acetonitrile / 0.17 h / 0 °C / Inert atmosphere

2.1: acetyl chloride / 4.5 h / 0 - 50 °C / Inert atmosphere

3.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 6 h / 760.05 Torr

4.1: lithium hydroxide monohydrate; water / d⁽⁴⁾-methanol; tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

5.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

5.2: 12 h / 20 °C / Inert atmosphere

6.1: trifluoroacetic acid / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

7.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

7.2: 12 h / 20 °C / Inert atmosphere

With lithium hydroxide monohydrate; palladium 10% on activated carbon; boron trifluoride diethyl etherate; water; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; acetyl chloride; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; d⁽⁴⁾-methanol; ethyl acetate; acetonitrile;
DOI:10.1002/anie.201304239

Reference yield:

: 1469300-25-1
C₁₃H₁₄N₄O₂

: 1469300-13-7
C₄₄H₅₈N₁₀O₁₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: acetyl chloride / 4.5 h / 0 - 50 °C / Inert atmosphere

2.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 6 h / 760.05 Torr

3.1: lithium hydroxide monohydrate; water / d⁽⁴⁾-methanol; tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

4.2: 12 h / 20 °C / Inert atmosphere

5.1: trifluoroacetic acid / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

6.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

6.2: 12 h / 20 °C / Inert atmosphere

With lithium hydroxide monohydrate; palladium 10% on activated carbon; water; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; acetyl chloride; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; d⁽⁴⁾-methanol; ethyl acetate;
DOI:10.1002/anie.201304239