2-(4-dimethylaminobenzylidene)amino-2-deoxy-1,3,4,6-tetra-O-acetyl-β-D-glucopyranose

Base Information

Chemical Name:2-(4-dimethylaminobenzylidene)amino-2-deoxy-1,3,4,6-tetra-O-acetyl-β-D-glucopyranose
CAS No.:1438624-41-9
Molecular Formula:C₂₃H₃₀N₂O₉
Molecular Weight:478.499
Hs Code.:

Synonyms:2-(4-dimethylaminobenzylidene)amino-2-deoxy-1,3,4,6-tetra-O-acetyl-β-D-glucopyranose

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Chemical Property of 2-(4-dimethylaminobenzylidene)amino-2-deoxy-1,3,4,6-tetra-O-acetyl-β-D-glucopyranose

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Technology Process of 2-(4-dimethylaminobenzylidene)amino-2-deoxy-1,3,4,6-tetra-O-acetyl-β-D-glucopyranose

There total 4 articles about 2-(4-dimethylaminobenzylidene)amino-2-deoxy-1,3,4,6-tetra-O-acetyl-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 5432-46-2,10034-19-2,10034-20-5,34948-62-4,110253-00-4,1191127-63-5
1,3,4,6-tetra-O-acetyl-D-glucosamine hydrochloride

: 100-10-7
4-dimethylamino-benzaldehyde

: 1438624-41-9
2-(4-dimethylaminobenzylidene)amino-2-deoxy-1,3,4,6-tetra-O-acetyl-β-D-glucopyranose

Guidance literature:: With piperidine; sodium acetate; In ethanol; for 0.0166667h; Reagent/catalyst; Time; Reflux;
DOI:10.2174/1570178611310020003

Reference yield:

: 14131-62-5
D-glucosamine hydrochloride

: 1438624-41-9
2-(4-dimethylaminobenzylidene)amino-2-deoxy-1,3,4,6-tetra-O-acetyl-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide / 2 h

2: pyridine / 12 h / 0 °C

3: hydrogenchloride / acetone; water / 0.5 h

4: sodium acetate; piperidine / ethanol / 0.02 h / Reflux

With piperidine; pyridine; hydrogenchloride; sodium acetate; sodium hydroxide; In ethanol; water; acetone;
DOI:10.2174/1570178611310020003

Reference yield:

: 51471-40-0
6-(hydroxymethyl)-3-[4-methoxybenzylideneamino]tetrahydropyran-2,4,5-triol

: 1438624-41-9
2-(4-dimethylaminobenzylidene)amino-2-deoxy-1,3,4,6-tetra-O-acetyl-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 12 h / 0 °C

2: hydrogenchloride / acetone; water / 0.5 h

3: sodium acetate; piperidine / ethanol / 0.02 h / Reflux

With piperidine; pyridine; hydrogenchloride; sodium acetate; In ethanol; water; acetone;
DOI:10.2174/1570178611310020003