2,6-di-tert-butyloxy-4-[(diisopropoxyphosphoryl)methoxy]-5-phenylpyrimidine

Base Information

Chemical Name:2,6-di-tert-butyloxy-4-[(diisopropoxyphosphoryl)methoxy]-5-phenylpyrimidine
CAS No.:1193313-40-4
Molecular Formula:C₂₅H₃₉N₂O₆P
Molecular Weight:494.568
Hs Code.:

Synonyms:2,6-di-tert-butyloxy-4-[(diisopropoxyphosphoryl)methoxy]-5-phenylpyrimidine

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Chemical Property of 2,6-di-tert-butyloxy-4-[(diisopropoxyphosphoryl)methoxy]-5-phenylpyrimidine

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Technology Process of 2,6-di-tert-butyloxy-4-[(diisopropoxyphosphoryl)methoxy]-5-phenylpyrimidine

There total 1 articles about 2,6-di-tert-butyloxy-4-[(diisopropoxyphosphoryl)methoxy]-5-phenylpyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1193313-38-0
5-bromo-2,6-di-tert-butyloxy-4-[(diisopropoxyphosphoryl)methoxy]pyrimidine

: 98-80-6
phenylboronic acid

: 1193313-40-4
2,6-di-tert-butyloxy-4-[(diisopropoxyphosphoryl)methoxy]-5-phenylpyrimidine

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In water; N,N-dimethyl-formamide; at 130 ℃; for 6h; Inert atmosphere;
DOI:10.1016/j.tet.2009.08.039

Reference yield: 23.0%

: 1193313-40-4
2,6-di-tert-butyloxy-4-[(diisopropoxyphosphoryl)methoxy]-5-phenylpyrimidine

: C₁₁H₉N₂O₆P^(2-)*2Li⁽¹⁺⁾

Guidance literature:: 2,6-di-tert-butyloxy-4-[(diisopropoxyphosphoryl)methoxy]-5-phenylpyrimidine; With trimethylsilyl bromide; In acetonitrile; at 20 ℃;

With triethylamine carbonate; In water; at 0 ℃;

In water;
DOI:10.1016/j.tet.2009.08.039