cyclo<-L-Phenylalanyl-D-prolyl-L-phenylalanyl-L-alanyl-O-(β-D-galactopyranosyl)-(1-4)-(2-desoxy-α-D-arabino-hexopyranosyl)-(1-6)-L-(2-amino-6-hydroxy)-caproyl-L-phenylalanyl->

Base Information

Chemical Name:cyclo<-L-Phenylalanyl-D-prolyl-L-phenylalanyl-L-alanyl-O-(β-D-galactopyranosyl)-(1-4)-(2-desoxy-α-D-arabino-hexopyranosyl)-(1-6)-L-(2-amino-6-hydroxy)-caproyl-L-phenylalanyl->
CAS No.:134262-53-6
Molecular Formula:C₅₃H₇₀N₆O₁₆
Molecular Weight:1047.17
Hs Code.:

cyclo<-L-Phenylalanyl-D-prolyl-L-phenylalanyl-L-alanyl-O-(β-D-galactopyranosyl)-(1-4)-(2-desoxy-α-D-arabino-hexopyranosyl)-(1-6)-L-(2-amino-6-hydroxy)-caproyl-L-phenylalanyl->

Synonyms:cyclo<-L-Phenylalanyl-D-prolyl-L-phenylalanyl-L-alanyl-O-(β-D-galactopyranosyl)-(1-4)-(2-desoxy-α-D-arabino-hexopyranosyl)-(1-6)-L-(2-amino-6-hydroxy)-caproyl-L-phenylalanyl->

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cyclo<-L-Phenylalanyl-D-prolyl-L-phenylalanyl-L-alanyl-O-(β-D-galactopyranosyl)-(1-4)-(2-desoxy-α-D-arabino-hexopyranosyl)-(1-6)-L-(2-amino-6-hydroxy)-caproyl-L-phenylalanyl->

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Technology Process of cyclo<-L-Phenylalanyl-D-prolyl-L-phenylalanyl-L-alanyl-O-(β-D-galactopyranosyl)-(1-4)-(2-desoxy-α-D-arabino-hexopyranosyl)-(1-6)-L-(2-amino-6-hydroxy)-caproyl-L-phenylalanyl->

There total 4 articles about cyclo<-L-Phenylalanyl-D-prolyl-L-phenylalanyl-L-alanyl-O-(β-D-galactopyranosyl)-(1-4)-(2-desoxy-α-D-arabino-hexopyranosyl)-(1-6)-L-(2-amino-6-hydroxy)-caproyl-L-phenylalanyl-> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 134262-50-3
cyclo<-L-Phenylalanyl-D-prolyl-L-phenylalanyl-L-alanyl-O-(2',3',4',6'-tetra-O-acetyl-β-D-galactopyranosyl)-(1-4)-(3,6-di-O-acetyl-2-desoxy-α-D-arabino-hexopyranosyl)-(1-6)-L-(2-amino-6-hydroxy)caproyl-L-phenylalanyl->

: 134262-53-6
cyclo<-L-Phenylalanyl-D-prolyl-L-phenylalanyl-L-alanyl-O-(β-D-galactopyranosyl)-(1-4)-(2-desoxy-α-D-arabino-hexopyranosyl)-(1-6)-L-(2-amino-6-hydroxy)-caproyl-L-phenylalanyl->

Guidance literature:: With potassium cyanide; In methanol; ethanol; for 12h;

Reference yield:

: 51450-24-9
hexa-O-acetyl-D-lactal

: 134262-53-6
cyclo<-L-Phenylalanyl-D-prolyl-L-phenylalanyl-L-alanyl-O-(β-D-galactopyranosyl)-(1-4)-(2-desoxy-α-D-arabino-hexopyranosyl)-(1-6)-L-(2-amino-6-hydroxy)-caproyl-L-phenylalanyl->

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / N-iodosuccinimide / acetonitrile / 144 h / 40 °C

2: 86 percent / H₂ / Raney-nickel / aq. ethanol / 7 h / Ambient temperature; other condition: NiCl₂*6H₂O, H₃BO₃, NaBH₄, EtOH, CH₂Cl₂, 2 h, room temperature

3: 97 percent / KCN / methanol; ethanol / 12 h

With potassium cyanide; N-iodo-succinimide; hydrogen; nickel; In methanol; ethanol; acetonitrile;

Reference yield:

: 134262-47-8
cyclo<-L-Phenylalanyl-D-prolyl-L-phenylalanyl-L-alanyl-O-(2',3',4',6'-tetra-O-acetyl-β-D-galactopyranosyl)-(1-4)-O-(3,6-di-O-acetyl-2-desoxy-2-iod-α-D-mannopyranosyl)-(1-6)-L-(2-amino-6-hydroxy)caproyl-L-phenylalanyl->

: 134262-53-6
cyclo<-L-Phenylalanyl-D-prolyl-L-phenylalanyl-L-alanyl-O-(β-D-galactopyranosyl)-(1-4)-(2-desoxy-α-D-arabino-hexopyranosyl)-(1-6)-L-(2-amino-6-hydroxy)-caproyl-L-phenylalanyl->

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / H₂ / Raney-nickel / aq. ethanol / 7 h / Ambient temperature; other condition: NiCl₂*6H₂O, H₃BO₃, NaBH₄, EtOH, CH₂Cl₂, 2 h, room temperature

2: 97 percent / KCN / methanol; ethanol / 12 h

With potassium cyanide; hydrogen; nickel; In methanol; ethanol;