endo-2-phenyl-exo-3,4,5-trithiatricyclo<5.2.1.0^2,6>decane

Base Information

• Chemical Name: endo-2-phenyl-exo-3,4,5-trithiatricyclo<5.2.1.0^2,6>decane
• CAS No.: 109909-04-8
• Molecular Formula: C₁₃H₁₄S₃
• Molecular Weight: 266.452

Synonyms:endo-2-phenyl-exo-3,4,5-trithiatricyclo<5.2.1.0^2,6>decane

Chemical Property of endo-2-phenyl-exo-3,4,5-trithiatricyclo<5.2.1.0^2,6>decane

Chemical Property:

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Technology Process of endo-2-phenyl-exo-3,4,5-trithiatricyclo<5.2.1.0^2,6>decane

There total 1 articles about endo-2-phenyl-exo-3,4,5-trithiatricyclo<5.2.1.0^2,6>decane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

2-phenylnorborn-2-ene (4237-08-5) → endo-2-phenyl-exo-3,4,5-trithiatricyclo<5.2.1.02,6>decane (109909-04-8)

Guidance literature:

With sulfur; 2,6-di-tert-butyl-4-methyl-phenol; In N,N-dimethyl-formamide; at 100 ℃; for 12h;

DOI:10.1021/jo00231a020

Reference yield: 88.0%

endo-2-phenyl-exo-3,4,5-trithiatricyclo<5.2.1.02,6>decane (109909-04-8) → 2-phenylnorbornane-2,3-dithiol (116376-55-7)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; at 25 ℃; for 15h;

DOI:10.1021/ja00230a037

Reference yield: 71.0%

endo-2-phenyl-exo-3,4,5-trithiatricyclo<5.2.1.02,6>decane (109909-04-8) → 2-phenylnorborn-2-ene (4237-08-5) + 3,4,5-trithiatricyclo<5.2.1.02,6>dec-8-ene (109958-15-8)

Guidance literature:

With bicyclo[2.2.1]hepta-2,5-diene; In benzene; at 102 ℃; for 6h;

DOI:10.1021/ja00230a037

upstream raw materials:

2-phenylnorborn-2-ene

Downstream raw materials:

2-phenylnorborn-2-ene

(1S,2S,6R,7R)-3,4,5-Trithia-tricyclo[5.2.1.0^2,6]dec-8-ene-8-carboxylic acid methyl ester

(1S,2R,6R,7R)-3,4,5-Trithia-tricyclo[5.2.1.0^2,6]dec-8-ene-2-carboxylic acid methyl ester

(1R,2R,6R,7S)-3,4,5-Trithia-tricyclo[5.2.1.0^2,6]decane-2-carboxylic acid methyl ester

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