(E)-but-2-en-1-yl 2,4-dimethoxybenzenesulfonate

Base Information

• Chemical Name: (E)-but-2-en-1-yl 2,4-dimethoxybenzenesulfonate
• CAS No.: 1590412-96-6
• Molecular Formula: C₁₂H₁₆O₅S
• Molecular Weight: 272.322
• Mol file: 1590412-96-6.mol

Synonyms:(E)-but-2-en-1-yl 2,4-dimethoxybenzenesulfonate

Chemical Property of (E)-but-2-en-1-yl 2,4-dimethoxybenzenesulfonate

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of (E)-but-2-en-1-yl 2,4-dimethoxybenzenesulfonate

There total 1 articles about (E)-but-2-en-1-yl 2,4-dimethoxybenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

(E)-but-2-enol (504-61-0,542-72-3) + 2,4-dimethoxybenzenesulfonylchloride (63624-28-2) → (E)-but-2-en-1-yl 2,4-dimethoxybenzenesulfonate (1590412-96-6)

Guidance literature:

(E)-but-2-enol; With potassium hydride; In tetrahydrofuran; hexane; at -78 ℃;

2,4-dimethoxybenzenesulfonylchloride; In tetrahydrofuran; hexane; at -78 ℃; for 48h;

DOI:10.1021/jo500394u

Reference yield: 36.0%

(E)-but-2-en-1-yl 2,4-dimethoxybenzenesulfonate (1590412-96-6) + tetraethylammoniumcyanide (13435-20-6) → 3-Pentenenitrile (16529-66-1)

Guidance literature:

In diethyl ether; acetonitrile; at 20 ℃;

DOI:10.1021/jo500394u

upstream raw materials:

(E)-but-2-enol

2,4-dimethoxybenzenesulfonylchloride

Downstream raw materials:

3-Pentenenitrile