Technology Process of C18H18O6
There total 8 articles about C18H18O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium dodecanethiolate;
In
N,N-dimethyl-formamide;
at 80 ℃;
for 5h;
DOI:10.1021/ol070929p
- Guidance literature:
-
Multi-step reaction with 8 steps
1: pyridine / 4 h / 20 °C
2: triethylorthoformate; tetrabutylammonium tribromide / 1 h / 20 °C
3: 5.00 g / K2CO3 / methanol / 1 h / 20 °C
4: 100 percent / K2CO3 / acetone / 14 h / Heating
5: tetrahydrofuran / 0.25 h / -20 °C
6: 7.53 g / aq. HCl / tetrahydrofuran / 2 h / 0 °C
7: modified chiral Rovis catalyst; Et3N / toluene / 12 h / 20 °C
8: sodium dodecanethiolate / dimethylformamide / 5 h / 80 °C
With
pyridine; hydrogenchloride; tetra-N-butylammonium tribromide; potassium carbonate; triethylamine; orthoformic acid triethyl ester;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1021/ol070929p
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 100 percent / K2CO3 / acetone / 14 h / Heating
2: tetrahydrofuran / 0.25 h / -20 °C
3: 7.53 g / aq. HCl / tetrahydrofuran / 2 h / 0 °C
4: modified chiral Rovis catalyst; Et3N / toluene / 12 h / 20 °C
5: sodium dodecanethiolate / dimethylformamide / 5 h / 80 °C
With
hydrogenchloride; potassium carbonate; triethylamine;
In
tetrahydrofuran; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1021/ol070929p
