2,3,4,6-tetra-O-acetyl-N-<(8-benzyloxycarbonylamino)octanoyl>-β-D-mannopyranosylamine

Base Information

Chemical Name:2,3,4,6-tetra-O-acetyl-N-<(8-benzyloxycarbonylamino)octanoyl>-β-D-mannopyranosylamine
CAS No.:74761-69-6
Molecular Formula:C₃₀H₄₂N₂O₁₂
Molecular Weight:622.67
Hs Code.:

Synonyms:2,3,4,6-tetra-O-acetyl-N-<(8-benzyloxycarbonylamino)octanoyl>-β-D-mannopyranosylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3,4,6-tetra-O-acetyl-N-<(8-benzyloxycarbonylamino)octanoyl>-β-D-mannopyranosylamine

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Technology Process of 2,3,4,6-tetra-O-acetyl-N-<(8-benzyloxycarbonylamino)octanoyl>-β-D-mannopyranosylamine

There total 3 articles about 2,3,4,6-tetra-O-acetyl-N-<(8-benzyloxycarbonylamino)octanoyl>-β-D-mannopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 41355-50-4
1-amino-2,3,4,6-tetra-O-acetyl-β-D-mannopyranosyl

: 74761-68-5
8-(benzyloxycarbonylamino)octanoyl chloride

: 74761-69-6
2,3,4,6-tetra-O-acetyl-N-<(8-benzyloxycarbonylamino)octanoyl>-β-D-mannopyranosylamine

Guidance literature:: With dmap; In dichloromethane; for 1h; Ambient temperature;
DOI:10.1016/S0008-6215(00)85529-9

Reference yield:

: 83-87-4,604-68-2,604-69-3,2152-77-4,4026-35-1,4163-59-1,4163-60-4,4163-61-5,4163-65-9,4257-94-7,4257-96-9,16299-15-3,19186-39-1,19189-55-0,25878-60-8,25941-03-1,32445-48-0,32445-49-1,32445-53-7,32445-54-8,34685-58-0,34685-59-1,43168-42-9,43168-44-1,43169-22-8,43169-25-1,66966-07-2,70749-17-6,80184-01-6,93221-01-3,93221-02-4,99630-88-3,109215-53-4,115792-70-6,115792-73-9,139894-92-1,139973-25-4,144071-49-8,147648-81-5
D-Mannose pentaacetate

: 74761-69-6
2,3,4,6-tetra-O-acetyl-N-<(8-benzyloxycarbonylamino)octanoyl>-β-D-mannopyranosylamine

Guidance literature:: Multi-step reaction with 3 steps

1: stannic tetrachloride / CH₂Cl₂ / 6 h

2: 61 percent / H₂ / Raney nickel / ethyl acetate / 6.5 h

3: 89 percent / 4-(dimethylamino)pyridine / CH₂Cl₂ / 1 h / Ambient temperature

With dmap; hydrogen; tin(IV) chloride; nickel; In dichloromethane; ethyl acetate;
DOI:10.1016/S0008-6215(00)85529-9

Reference yield:

: 53784-29-5
2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl azide

: 74761-69-6
2,3,4,6-tetra-O-acetyl-N-<(8-benzyloxycarbonylamino)octanoyl>-β-D-mannopyranosylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / H₂ / Raney nickel / ethyl acetate / 6.5 h

2: 89 percent / 4-(dimethylamino)pyridine / CH₂Cl₂ / 1 h / Ambient temperature

With dmap; hydrogen; nickel; In dichloromethane; ethyl acetate;
DOI:10.1016/S0008-6215(00)85529-9