(2S,4R)-1-(4-methylphenylsulfonyl)-4-[(E)-2-phenyl-1-ethenyl]-2-[(E)-2-phenyl-1-ethenylsulfanylmethyl]pyrrolidine

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Chemical Name:(2S,4R)-1-(4-methylphenylsulfonyl)-4-[(E)-2-phenyl-1-ethenyl]-2-[(E)-2-phenyl-1-ethenylsulfanylmethyl]pyrrolidine
CAS No.:677736-97-9
Molecular Formula:C₂₈H₂₉NO₂S₂
Molecular Weight:475.676
Hs Code.:

Synonyms:(2S,4R)-1-(4-methylphenylsulfonyl)-4-[(E)-2-phenyl-1-ethenyl]-2-[(E)-2-phenyl-1-ethenylsulfanylmethyl]pyrrolidine

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Chemical Property of (2S,4R)-1-(4-methylphenylsulfonyl)-4-[(E)-2-phenyl-1-ethenyl]-2-[(E)-2-phenyl-1-ethenylsulfanylmethyl]pyrrolidine

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Technology Process of (2S,4R)-1-(4-methylphenylsulfonyl)-4-[(E)-2-phenyl-1-ethenyl]-2-[(E)-2-phenyl-1-ethenylsulfanylmethyl]pyrrolidine

There total 1 articles about (2S,4R)-1-(4-methylphenylsulfonyl)-4-[(E)-2-phenyl-1-ethenyl]-2-[(E)-2-phenyl-1-ethenylsulfanylmethyl]pyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66680-87-3,66680-88-4,79159-76-5
(2-phenylvinyl)tributylstannane

: (S)-4-Iodo-2-((Z)-styrylsulfanylmethyl)-1-(toluene-4-sulfonyl)-pyrrolidine

: (2S,4R)-1-(4-methylphenylsulfonyl)-4-[(E)-2-phenyl-1-ethenyl]-2-[(Z)-2-phenyl-1-ethenylsulfanylmethyl]pyrrolidine

: 677736-97-9
(2S,4R)-1-(4-methylphenylsulfonyl)-4-[(E)-2-phenyl-1-ethenyl]-2-[(E)-2-phenyl-1-ethenylsulfanylmethyl]pyrrolidine

Guidance literature:: With 1,1'-azobis(1-cyanocyclohexanenitrile); In toluene; at 105 - 110 ℃; for 4h;
DOI:10.1021/ja031766c

Reference yield: 74.0%

: 677736-97-9
(2S,4R)-1-(4-methylphenylsulfonyl)-4-[(E)-2-phenyl-1-ethenyl]-2-[(E)-2-phenyl-1-ethenylsulfanylmethyl]pyrrolidine

: (2S,4R)-1-(4-methylphenylsulfonyl)-4-[(E)-2-phenyl-1-ethenyl]-2-[(E)-2-phenyl-1-ethenylsulfinylmethyl]pyrrolidine

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In ethyl acetate; at -40 - -30 ℃; for 1.5h;
DOI:10.1021/ja031766c

Reference yield:

: 677736-97-9
(2S,4R)-1-(4-methylphenylsulfonyl)-4-[(E)-2-phenyl-1-ethenyl]-2-[(E)-2-phenyl-1-ethenylsulfanylmethyl]pyrrolidine

: (2S,4R)-1-(4-methylphenylsulfonyl)-4-[(E)-2-phenyl-1-ethenyl]-2-pyrrolidinecarbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / mCPBA / ethyl acetate / 1.5 h / -40 - -30 °C

2: 92 percent / 2,6-lutidine; TFAA / CH₂Cl₂ / 2 h / -25 °C

With 2,6-dimethylpyridine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic anhydride; In dichloromethane; ethyl acetate;
DOI:10.1021/ja031766c