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C16H13BrO2

Base Information
  • Chemical Name:C16H13BrO2
  • CAS No.:1314806-80-8
  • Molecular Formula:C16H13BrO2
  • Molecular Weight:317.182
  • Hs Code.:
C<sub>16</sub>H<sub>13</sub>BrO<sub>2</sub>

Synonyms:C16H13BrO2

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Chemical Property of C16H13BrO2
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Technology Process of C16H13BrO2

There total 1 articles about C16H13BrO2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
1-Bromo-2-iodobenzene; With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; for 0.166667h; Inert atmosphere;
1-Ethynyl-3,5-dimethoxy-benzene; With triethylamine; for 12.0833h; Inert atmosphere;
DOI:10.1039/c6cc03414d
Guidance literature:
C16H13BrO2; With n-butyllithium; In diethyl ether; hexane; at -78 - -40 ℃; for 2h; Inert atmosphere;
Triisopropyl borate; In diethyl ether; hexane; at -78 - 20 ℃; for 16h; Inert atmosphere;
DOI:10.1039/c8cc05743e

Reference yield: 45.0%

Guidance literature:
C16H13BrO2; With n-butyllithium; In diethyl ether; hexane; at -78 - -40 ℃; for 2h; Inert atmosphere;
With Triisopropyl borate; In diethyl ether; hexane; at -78 - 20 ℃; for 16h; Inert atmosphere;
DOI:10.1039/c6cc03414d
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