β-alanine, N-<α-methyl-N-<<(2-methylcyclohexyl)oxy>carbonyl>-L-tryptophyl>-D-3-(phenylmethyl)-, phenylmethyl ester, (1R-trans)

Base Information

Chemical Name:β-alanine, N-<α-methyl-N-<<(2-methylcyclohexyl)oxy>carbonyl>-L-tryptophyl>-D-3-(phenylmethyl)-, phenylmethyl ester, (1R-trans)
CAS No.:146566-62-3
Molecular Formula:C₃₇H₄₃N₃O₅
Molecular Weight:609.766
Hs Code.:

Synonyms:β-alanine, N-<α-methyl-N-<<(2-methylcyclohexyl)oxy>carbonyl>-L-tryptophyl>-D-3-(phenylmethyl)-, phenylmethyl ester, (1R-trans)

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Chemical Property of β-alanine, N-<α-methyl-N-<<(2-methylcyclohexyl)oxy>carbonyl>-L-tryptophyl>-D-3-(phenylmethyl)-, phenylmethyl ester, (1R-trans)

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Technology Process of β-alanine, N-<α-methyl-N-<<(2-methylcyclohexyl)oxy>carbonyl>-L-tryptophyl>-D-3-(phenylmethyl)-, phenylmethyl ester, (1R-trans)

There total 4 articles about β-alanine, N-<α-methyl-N-<<(2-methylcyclohexyl)oxy>carbonyl>-L-tryptophyl>-D-3-(phenylmethyl)-, phenylmethyl ester, (1R-trans) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19043-03-9
(1R,2R)-(-)-trans-2-methylcyclohexanol

: 146566-62-3
β-alanine, N-<α-methyl-N-<<(2-methylcyclohexyl)oxy>carbonyl>-L-tryptophyl>-D-3-(phenylmethyl)-, phenylmethyl ester, (1R-trans)

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) pyridine, 2.) Et₃N / 1.) CH₂Cl₂, 0 deg C, 1 h, 2.) THF, RT, 3 h

2: 96 percent / aq. LiOH / dioxane / 36 h / Ambient temperature

3: 1.) pentafluorophenol, N,N'-dicyclohexylcarbodiimide / 1.) EtOAc, 0 deg C, 4 h, 2.) EtOAc, 0 deg C, 16 h

With pyridine; lithium hydroxide; 2,3,4,5,6-pentafluorophenol; triethylamine; dicyclohexyl-carbodiimide; In 1,4-dioxane;
DOI:10.1021/jm00057a005

Reference yield:

: 142854-50-0
L-α-methyl-tryptophan methyl ester

: 146566-62-3
β-alanine, N-<α-methyl-N-<<(2-methylcyclohexyl)oxy>carbonyl>-L-tryptophyl>-D-3-(phenylmethyl)-, phenylmethyl ester, (1R-trans)

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) pyridine, 2.) Et₃N / 1.) CH₂Cl₂, 0 deg C, 1 h, 2.) THF, RT, 3 h

2: 96 percent / aq. LiOH / dioxane / 36 h / Ambient temperature

3: 1.) pentafluorophenol, N,N'-dicyclohexylcarbodiimide / 1.) EtOAc, 0 deg C, 4 h, 2.) EtOAc, 0 deg C, 16 h

With pyridine; lithium hydroxide; 2,3,4,5,6-pentafluorophenol; triethylamine; dicyclohexyl-carbodiimide; In 1,4-dioxane;
DOI:10.1021/jm00057a005

Reference yield:

: (1R-trans)-α-methyl-N-<<(2-methylcyclohexyl)oxy>carbonyl>-L-tryptophan methyl ester

: 146566-62-3
β-alanine, N-<α-methyl-N-<<(2-methylcyclohexyl)oxy>carbonyl>-L-tryptophyl>-D-3-(phenylmethyl)-, phenylmethyl ester, (1R-trans)

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / aq. LiOH / dioxane / 36 h / Ambient temperature

2: 1.) pentafluorophenol, N,N'-dicyclohexylcarbodiimide / 1.) EtOAc, 0 deg C, 4 h, 2.) EtOAc, 0 deg C, 16 h

With lithium hydroxide; 2,3,4,5,6-pentafluorophenol; dicyclohexyl-carbodiimide; In 1,4-dioxane;
DOI:10.1021/jm00057a005