C₅₈H₄₀O₁₀P₄Rh₂W₂, triclinic

Base Information

Chemical Name:C₅₈H₄₀O₁₀P₄Rh₂W₂, triclinic
CAS No.:105335-70-4
Molecular Formula:C₅₈H₄₀O₁₀P₄Rh₂W₂
Molecular Weight:1594.36
Hs Code.:

C<sub>58</sub>H<sub>40</sub>O<sub>10</sub>P<sub>4</sub>Rh<sub>2</sub>W<sub>2</sub>, triclinic

Synonyms:C₅₈H₄₀O₁₀P₄Rh₂W₂, triclinic

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Chemical Property of C₅₈H₄₀O₁₀P₄Rh₂W₂, triclinic

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Technology Process of C₅₈H₄₀O₁₀P₄Rh₂W₂, triclinic

There total 2 articles about C₅₈H₄₀O₁₀P₄Rh₂W₂, triclinic which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.3%

: 105371-68-4
(CO)4W(P(C₆H₅)2)2Rh(C₈H₁₃)

: 105335-70-4
C₅₈H₄₀O₁₀P₄Rh₂W₂, triclinic

Guidance literature:: With carbon monoxide; In dichloromethane; soln. of the dinuclear complex in CH2Cl2 stirred at room temp. under atmosphere of CO (pressure 90 psi) for 4 h; gas was vented, solvent evapd., residue chromd. on basic alumina (eluant CH2Cl2/hexane (20/80)); elem. anal.; one more unidentified compound was formed;

Reference yield:

: ((CO)4W(P(C₆H₅)2)2Rh(CO)2)2

: 105335-70-4
C₅₈H₄₀O₁₀P₄Rh₂W₂, triclinic

Guidance literature:: In not given; removal of the solvent and the CO atmosphere from the solns. of the terminal CO containing complex; IR detection;

Reference yield:

: 105335-70-4
C₅₈H₄₀O₁₀P₄Rh₂W₂, triclinic

: 88904-48-7
(CO)4W(P(C₆H₅)2)2Rh(H)(CO)(P(C₆H₅)3)

Guidance literature:: With hydrogen; triphenylphosphine; carbon monoxide; In dichloromethane; vessel with CH2Cl2 soln. of the tetranuclear complex and PPh3 was pressurized to 100 psi of H2, after 30 min H2 was vented to 80 psi and vessel repressurized to 100 psi with CO for 30 min; not isolated (IR detection);