tert-butyl{(S)-2-[4-(4-methoxybenzyloxymethyl)phenyl]propoxy}diphenylsilane

Base Information

Chemical Name:tert-butyl{(S)-2-[4-(4-methoxybenzyloxymethyl)phenyl]propoxy}diphenylsilane
CAS No.:1333080-40-2
Molecular Formula:C₃₄H₄₀O₃Si
Molecular Weight:524.775
Hs Code.:

Synonyms:tert-butyl{(S)-2-[4-(4-methoxybenzyloxymethyl)phenyl]propoxy}diphenylsilane

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Chemical Property of tert-butyl{(S)-2-[4-(4-methoxybenzyloxymethyl)phenyl]propoxy}diphenylsilane

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Technology Process of tert-butyl{(S)-2-[4-(4-methoxybenzyloxymethyl)phenyl]propoxy}diphenylsilane

There total 9 articles about tert-butyl{(S)-2-[4-(4-methoxybenzyloxymethyl)phenyl]propoxy}diphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1333080-39-9
(S)-2-(4-(4-methoxybenzyloxy)phenyl)propan-1-ol

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1333080-40-2
tert-butyl{(S)-2-[4-(4-methoxybenzyloxymethyl)phenyl]propoxy}diphenylsilane

Guidance literature:: With 1H-imidazole; dmap; In dichloromethane; at 0 - 20 ℃; for 6h;
DOI:10.1016/j.tetasy.2011.06.019

Reference yield:

: 1333080-35-5
2-(4-((4-methoxybenzyloxy)methyl)phenyl)propan-1-ol

: 1333080-40-2
tert-butyl{(S)-2-[4-(4-methoxybenzyloxymethyl)phenyl]propoxy}diphenylsilane

Guidance literature:: Multi-step reaction with 3 steps

1: Burkholderia cepacia lipase-PS / di-isopropyl ether / 12 h / 20 °C / Molecular sieve; Enzymatic reaction

2: methanol; potassium carbonate

3: 1H-imidazole; dmap / dichloromethane / 6 h / 0 - 20 °C

With 1H-imidazole; methanol; dmap; Burkholderia cepacia lipase-PS; potassium carbonate; In dichloromethane; di-isopropyl ether;
DOI:10.1016/j.tetasy.2011.06.019

Reference yield:

: 1333080-33-3
1-(4-methoxybenzyloxymethyl)-4-isopropenylbenzene

: 1333080-40-2
tert-butyl{(S)-2-[4-(4-methoxybenzyloxymethyl)phenyl]propoxy}diphenylsilane

Guidance literature:: Multi-step reaction with 4 steps

1.1: dimethylsulfide borane complex / tetrahydrofuran / 4.25 h / 0 - 20 °C / Inert atmosphere

1.2: 1 h / 0 °C

2.1: Burkholderia cepacia lipase-PS / di-isopropyl ether / 12 h / 20 °C / Molecular sieve; Enzymatic reaction

3.1: methanol; potassium carbonate

4.1: 1H-imidazole; dmap / dichloromethane / 6 h / 0 - 20 °C

With 1H-imidazole; methanol; dmap; dimethylsulfide borane complex; Burkholderia cepacia lipase-PS; potassium carbonate; In tetrahydrofuran; dichloromethane; di-isopropyl ether;
DOI:10.1016/j.tetasy.2011.06.019