(+/-)-3,7-dimethyloct-6-enyl [4-(2-methyl-1,3-dioxolan-2-yl)phenyl]-2-oxoacetate

Base Information

Chemical Name:(+/-)-3,7-dimethyloct-6-enyl [4-(2-methyl-1,3-dioxolan-2-yl)phenyl]-2-oxoacetate
CAS No.:251538-31-5
Molecular Formula:C₂₂H₃₀O₅
Molecular Weight:374.477
Hs Code.:

Synonyms:(+/-)-3,7-dimethyloct-6-enyl [4-(2-methyl-1,3-dioxolan-2-yl)phenyl]-2-oxoacetate

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Chemical Property of (+/-)-3,7-dimethyloct-6-enyl [4-(2-methyl-1,3-dioxolan-2-yl)phenyl]-2-oxoacetate

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Technology Process of (+/-)-3,7-dimethyloct-6-enyl [4-(2-methyl-1,3-dioxolan-2-yl)phenyl]-2-oxoacetate

There total 4 articles about (+/-)-3,7-dimethyloct-6-enyl [4-(2-methyl-1,3-dioxolan-2-yl)phenyl]-2-oxoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 4360-68-3
2-(4-bromophenyl)-2-methyl-1,3-dioxolane

: 99559-01-0
bis(3,7-dimethylocta-6-enyl) ethane-1,2-dioate

: 251538-31-5
(+/-)-3,7-dimethyloct-6-enyl [4-(2-methyl-1,3-dioxolan-2-yl)phenyl]-2-oxoacetate

Guidance literature:: With magnesium; In tetrahydrofuran; at -78 ℃; for 0.5h;
DOI:10.1002/1522-2675(20000705)83:7<1645::AID-HLCA1645>3.0.CO;2-S

Reference yield:

: 99559-01-0
bis(3,7-dimethylocta-6-enyl) ethane-1,2-dioate

: 251538-31-5
(+/-)-3,7-dimethyloct-6-enyl [4-(2-methyl-1,3-dioxolan-2-yl)phenyl]-2-oxoacetate

Guidance literature:: With magnesium;

Reference yield:

: 106-22-9
Citronellol

: 251538-31-5
(+/-)-3,7-dimethyloct-6-enyl [4-(2-methyl-1,3-dioxolan-2-yl)phenyl]-2-oxoacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 43 percent / pyridine / 0.5 h / 0 °C

2: 58 percent / Mg / tetrahydrofuran / 0.5 h / -78 °C

With pyridine; magnesium; In tetrahydrofuran; 1: Acylation / 2: Grignard reaction;
DOI:10.1002/1522-2675(20000705)83:7<1645::AID-HLCA1645>3.0.CO;2-S